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Report Number.- 40554 QC Report : Method Blank Data Date : 10/19/2004 Project Name : Tesoro 67080 Project Number: D003-007 Method Method Measured Reporting Analysis Date Measured Reporting Analysis Date Parameter Value „ Emit Units Method Analyzed Parameter Value Limit Units Method Analyzed TPK as Diesel <50 50 ug1L M EPA 8015 10113/2004 Odacosane(Diesel Surrogate) 128 % M EPA 8015 10/13/2004 Benzene <0.50 0.50 uglL EPA 82608 10/1512004 Toluene <0.50 0.50 ug1L EPA 82608 10/15/2004 Ethylbenzene <0.50 0.50 ug1L EPA 82608 10/1512004 Total Xylenes <0.50 0.50 uVL EPA 8260B 10/1512004 Methyl-t-butyl ether(MTBE) <0.50 0.50 ug1L EPA 82608 10/1512004 Diisopmpyt ether(DIPE) <0.50 0.50 ug1L EPA 82608 10/1512004 Ethyl-l•butyl ether(ETRE) <0.50 0.50 ug1L EPA 8260B 1 011 512 0 04 Tert-amyl methyl ether(TAME) <0.50 0.50 uglL EPA 82608 10/1512004 Tert-Butanol <5.0 5.0 ug1L EPA 8260B 10/1512004 TPH as Gasoline <50 50 uglL EPA 8260E 1011512004 Toluene-d8(Surr) 98.4 % EPA 82606 10115/2004 4-Bromofluorobenzene(Surr) 107 % EPA 8260E 1 011 5120 04 Benzene <0.50 0.50 ug1L EPA 82608 10!1512004 Toluene - <0.50 0.50 ug1L EPA 82608 10/15/2004 Ethylbenzene <0.50 0.50 ug1L EPA 8260B 10115/2004 Total Xylenes <0.50 0.50 uglL EPA 8260B 1 011 512 004 Methyl-t-butyl ether(MTBE) <0.50 0.50 ugll- EPA 8260B 1 011 512 0 04 Diisopropyl ether(DIPE) <0.50 0.50 ug1L EPA 82608 10/1512004 Ethyl-t-butyl ether(ETBE) <0.50 0.50 uglL EPA 8260B 10115/2004 Teri-amyl methyl ether(TAME) <0.50 0.50 ug1L EPA 8260B 1 011 512 0 04 Terl-Butanol <5.0 5.0 uglL EPA 82608 10/1512004 TPH as Gasoline <50 50 uglL EPA 8260B 10/1512004 Toluene-dB(Surr) 102 % EPA 8260B 1 011 512 0 04 4-Bromofluorobenzene(Surr) 92.0 % EPA 8260B 10115120134 i Approved By: Jo f iff KIFF ANALYTICAL, LLC 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800