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05/19/2003 08:25 2094671118 AGE STOCKTON PAGE 05 <br />May 14 2003 11:07AM CRMP13 LL ANALYTICAL 1 5-79B-1620 p.5 <br />McCampbel) Analytical inc. <br />110 � � 925��i620 Fwt; 915-798.1 2.2 <br />b r/lwww,tac bell.com ]yneiL qutn mebell core <br />Advanced GeoEnvironmental, Tnc_ Client Project ID; Flag City Chevron Date Sampled: 05/07/03 <br />837 Sbaw Road DateRecci-vud: 05/08/03 <br />Stogy CA 95215 Client Contact: Tim Q ellar bate Bxtracu:d: 05/08/03 <br />Client P.O-. Date A alyztd; 05/08/03-05/ld/03 <br />Gas*Uue Range (C6-C12) Volatile Hydrocarbons as Gasoline with BTEX clad MTBE" <br />Extracdopmethod: 9W50309 ACAlytiealmarlteds, 9W80213/8015Ctn W-ork0rcim 03M24 <br />Lab ID Client li? Matrix TPH(y) MTHE Benzene Toluene Ethylbarrur o Xylenes <br />001A DSP-1 S 9.l,b,m 0.0067 0.051 0.056 0,013 I 90.4 <br />OD2A DSP-2 S 2,9,a ND 0.061 0.037 0.23 1 87.1 <br />003A DSP-3 S ].9,V ND 0,0066 ND ND [ 89.6 <br />004A DSPC S 170,b,m NDc0.1 0.47 NDa01 0,50 20 ..# <br />005A DSP-5 S i7,g,m ..� NDc0.01 0.20 - — 0,080 0.57 2 89.9 <br />006A L)Sp_6 S ND ND ND ND ND 1 889 <br />007A PL-1 9 ND _._ ND ND ND ND l 95,0 <br />OO&A PLr2 S ND __ NO ND ND ND 1 88,7 <br />009APL3 S 2.4,g ND 0.4060 ND ND 1 910 <br />010A PL-4 5 3.7,g,tr1 Nb 0.015 ND 0.031 1 104 <br />011A FL-5 9 ND ND NA ND NO 1 93.8 <br />012A - PL-6 S ND �. ND NOI+1D <br />NO 1 96.4 <br />013A STK-1 S ND NO ND <br />ND _ NA i 111 <br />014A STK-2 5 N-D ND Nb ND NO I .i. 109 <br />RcPor�+g Lath for DF -1; yy NA NA NA <br />ND nets not detected at tmr NA NA i uglL <br />strove tlro rcportina ]iodt S 1.0 0.05 0.005 0,005 0.005 0.005 1 mg/l�g <br />"water and vapor samples are reported in µg/L, soil Rod sludpa samples in mg/kg, wipe samples in ug/wipe, and TCLP vxt:acts In 4g/L. <br /># cluttered ohreartatogram; sample peak Coelutes with surrogate peak, <br />+The following descriptions of tht TPH chromatogram are cursory in nature and McCamphetl Apaly4ic2) is not reaponsfbk: for their int®rpretation_ a) <br />unmodified or weekly modified gasoline is significant; b) heavier gasoltnc range compounds are sip ficant(agod gawlioe2); c) tighter panto range <br />compotlttea Rhe most mobile $action) are significant; d) gasoline range compounds' having broad chromatographic peeks Ore sign scant; biologically <br />Wltarod gasoline?; e) TPH pattem that does bat appear to be derived from. gasoline (stoddard solvent / mineral spirit?); f) on.3 to a few isolated non-tweet <br />peaks present; g) 6tron61y aged gasoline or diesel range compounds are etgnificatlt; h) lighter than water inimiacible 8heen/lxroduct is pm4ent; t) liquid <br />sample that Contains greater than --2 vol, % sedimenc; j) reporting limit raisM due to higit MTBE content; k) TPII pattern khat does not appear to be <br />derived from gasolinic (aviation Bea), m) no recognizable pattern. <br />DHS Ceitififaation Na. 1644 Angela Aydelius, Lab Manager <br />