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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> http://www,mccam�beli.com E-mail:main@mccampbell.com- <br /> • <br /> ' Advanced GeoEnvironmental Client Project ID: Hess DuBios Date Sampled: 08/30/01 <br /> 837 Shaw Road Date Received: 09/05/01 <br /> Stockton,CA 95215 Client Contact: Bill Tittle Date Extracted: 09/12/01 <br /> Client P.O: Date Analyzed: 09/12/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab 1D 76961 <br /> Client 1D Pump Test/EW-1 <br /> Matrix W <br /> Rcpmng Limit Repotting Limit <br /> Compound Concentration* W S Compound Concentration* W S <br /> ' Acetone�b) ND 5.0 25 trans-1,3-Dichloropropene ND 1.0 5.0 <br /> Benzene ND 1.0 5.0 Ethylene dibromide ND 1.0 5.0 <br /> Bromobenzene ND 1.0 5.0 Ethylbenzene 4.4 1.0 5.0 <br /> Bromochloromethane ND LO 5.0 Hexachlorobutadiene ND 5.0 25 <br /> Bromodichlorometbane ND 1.0 5.0 Iodomethane ND 1.0 5.0 <br /> Bromaform ND L0 5.0 Isopropylbenzene 32 1.0 i 5.0 <br /> Bromomethane ND 1.0 5.0 p-lsopropyl toluene 5.7 1.0 5.0 <br /> n-Butyl benzene 7.6 1.0 5.0 Methyl butyl ketone ND 1.0 5.0 <br /> sec-Butyl benzene ND 1.0 5.0 Methylene Chloride` ND 1.0 5.0 <br /> tert-Butyl benzene 1.9 1.0 5.0 Methyl ethyl ketone ND 2.0 10 <br /> Carbon Disulfide ND LO 5.0 Methyl isobutyl ketone ND 1.0 5.0 <br /> Carbon Tetrachloride ND i.0 5.0 Methyl tert-Butyl Ether(MTBE) --- 1.0 5.0 <br /> ' Chlorobenzene ND 1.0 5.0 Naphthalene 20 5.0 5.0 <br /> Chloroethane ND 1.0 5.0 n-Propyl benzene 59 1.0 5.0 <br /> 2-Chloroethyl Vinyl Ether"' ND 1.0 5.0 Styrene ND 1.0 5.0 <br /> ' Chloroform ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0 <br /> Chloromethane ND 1.0 5.0 1,1,2,2-Tetrachloroethane ND 1.0 5.0 <br /> 2-Chlorotoluene ND 1.0 5.0 Tetrachloroethene ND 1.0 5.0 <br /> 4-Chlorotoluene ND 1.0 5.0 Toluene 8.3 1.0 5.0 <br /> ' Dibromochloromethane ND 1.0 5.0 1,2,3-Trichlorobenzene ND 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2.0 10 1,2,4-Trichlorobenzene ND 5.0 25 <br /> Dibromomethane ND 1.0 1 5.0 1,1,1-Trichloroetbane ND 1.0 5.0 <br /> 1,2-Dichlorobenzene 4.8 1.0 5.0 1,1,2-Trichloroethane ND 1.0 5.0 <br /> 1,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene ND Lo 5.0 <br /> 1,4-Dichlorobenzene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> Dichlorodifluoromethane ND 1.0 5.0 1,2,3-Trichloropropane ND 1.0 5.0 <br /> 1,1-Dichloroethane ND 1.0 5.0 1,2,4-Trimethylbenzene 26 1.0 5.0 <br /> 1,2-Dichloroethane ND 1.0 5.0 1,3,5-Trimethylben7ene 7.0 1.0 5.0 <br /> 1,1-Dichloroethene ND 1.0 5.0 Vinyl Acetate :d ND 5.0 25 <br /> cis-1,2-Dichloroethene 1.5 1.0 5.0 Vinyl Chloride a 1.1 1.0 5.0 <br /> trans-1,2-Dichloroethene ND 1.0 5.0 Xylenes,total 47 1.0 5.0 <br /> ' 1,2-Dichloropropane ND 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND i.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1.0 5.0 Dibromofluoromethane 109 <br /> 1,1-Dichloropropene ND 1.0 5.0 Toluene-d8 92 <br /> ' cis-1,3-Dichloropropane L ND I 1.0 5.0 4-Bromofluorobenzene 99 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b)2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> . pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than-5 vol.% <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />