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1 <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> hM://www.mccampbelf.com E-mail: main@mccatnpbell.com <br /> ' Advanced GeoEnvironmental Client Project ID: Hess&Dubios Date Sampled:05/02/01 <br /> 837 Shaw Road Date Received: 05/03/01 <br /> Stockton, CA 95215 Client Contact:Bill Little Date Extracted: 05/03/01 <br /> Client P.O: Date Analyzed: 05/03/01 <br /> tVolatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 66698 <br /> t Client ID MW10-050201 <br /> Matrix W <br /> Compound Concentration* Reporting Limit Compound Concentration* Reporting Limit <br /> tW S W S <br /> Acetone m) ND<60 5.0 25 trans-1,3-Dichloropropene ND<20 1.0 5.0 <br /> Benzene ND<20 1.0 5.0 Ethylene dibromide ND<20 1.0 5.0 <br /> Bromobenzene NIX20 1.0 5.0 Ethylbenzene ND<20 1.0 5.0 <br /> ' Bromochloromethane ND<20 1.0 5.0 Hexachlorobutadiene ND<20 5.0 25 <br /> Bromodichloromethane ND<20 1.0 5.0 Iodomethane ND<20 1.0 5.0 <br /> Bromoform ND<20 I.0 5.0 lsopropylbenzene ND<20 1.0 5.0 <br /> Bromomethane ND<20 1.0 5.0 p-Isopropyl toluene ND<20 1.0 5.0 <br /> ' n-Butyl benzene ND<20 1.0 5.0 Methyl butyl ketone ND<20 1.0 5.0 <br /> sec-Butyl benzene ND<20 1.0 5.0 Methylene Chloride"I ND<40 1.0 5.0 <br /> tert-Butyl benzene ND<20 1.0 5.0 Methyl ethyl ketone ND<20 2.0 10 <br /> Carbon Disulfide ND<20 1.0 5.0 Methyl isobutyl ketones ND<20 1.0 5.0 <br /> Carbon Tetrachloride ND<20 1.0 5.0 Methyl tert-Butyl Ether(MTBE) -- 1.0 5.0 <br /> Chlorobenzene ND<20 1.0 5.0 Naphthalene ND<20 5.0 5.0 <br /> Chloroethane ND<20 1.0 5.0 n-Propyl benzene ND<20 1.0 5.0 <br /> 2-Chloroethyl Vinyl Ethers` ND<20 1.0 5.D Styrene I ND<20 1.0 5.0 <br /> Chloroform ND<20 1.0 5.0 1,1,1,2-Tetrachloroethane ND<20 1.0 5.0 <br /> Chloromethane ND<20 1.0 5.0 1,1,2,2-Tetrachloroethane ND<20 1.0 5.0 <br /> 2-Chlorotolucne ND<20 1.0 5.0 Tetrachloroethene 400 1.0 5.0 <br /> 4-Chlorotoluene ND<20 1.0 5.0 Toluene ND<20 1.0 5.0 <br /> ' Dibromochloromethane ND<20 1.0 5.0 1,2,3-Trichlorobenzene ND<20 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND<20 2.0 10 1,2,4-Trichlorobenzenc ND<20 5.0 25 <br /> Dibromomethane ND<20 1.0 5.0 1,1,1-Trichloroethane ND<20 1.0 5.0 <br /> 1,2-Dichlorobenzene ND<20 1.0 5.0 1,1,2-Trichloroethane ND<20 1.0 5.0 <br /> ' 1,3-Dichlorobenzene ND<20 1.0 5.0 Trichloroethene 350 1.0 5.0 <br /> 1,4-Dichlorobenzene ND<20 1.0 5.0 Trichlorofluoromethane ND<20 1.0 5.0 <br /> Dichlorodifluoromethane ND<20 1.0 5.0 1,2,3-Trichloropropane ND<20 1.0 5.0 <br /> ' l,I-Dichloroethane ND<20 1.0 5.0 1,2,4-Trimethylbenzene ND<20 1.0 5.0 <br /> 1,2-Dichloroethane ND<20 1.0 5.0 1,3,5-Trimethylbenzene ND<20 1.0 5.0 <br /> I,1-Dichloroethane ND<20 1.0 5.0 Vinyl Acetate 'J ND<2015.0L-O <br /> cis-1,2-Dichloroethene 1200 1.0 5.0 Vinyl Chloride 11D trans-l,2-Dichloroethene ND<20 1.0 5.0 Xylenes,total ND<200 <br /> 1,2-Dichloropmpane ND<20 1.0 5.0 Comments: <br /> 1,3-Dichloropmpane ND<20 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<20 1.0 5.0 Dibromofluoromethane 111 <br /> ' l,I-Dichloropropene ND<20 1.0 5.0 Toluene-d8 97 <br /> cis-1,3-Dichloropropene ND<20 1.0 5.0 4-Bromofluorobenzene 103 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ' ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than .-5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,"Lab Director <br />