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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ' jo bttp /www -.a+ E-mail matn@mccampbell com <br /> • <br /> Advanced GeoEnvironmentaI Client Project ID Chase-Madison Date Sampled 11/03/98 <br /> 4005 North Wilson Way Date Received 11/06/98 <br /> ' Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 11/08/98 <br /> Client P O Date Analyzed 11/08/98 <br /> ' Volatile Organics By GC/MS <br /> BPA method 8260 <br /> Lab ID 98243 <br /> ' Client ID MW-1/11-3-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<2 Ethylbenzene ND <br /> Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND Iodomethane ND <br /> Bromochloromethane ND Isopropylbenzene ND <br /> ' Bromodichloromethane ND p-Isopropyl toluene ND <br /> Bromoform ND Methyl butyl ketone ND <br /> Bromomethane ND Methylene Chloride(') ND <br /> n-Butyl benzene ND Methyl ethyl ketone ND <br /> ' sec-Butyl benzene ND Methyl isobutyl ketone a ND <br /> tert Butyl benzene ND Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND Napthalene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> Chlorobenzene ND Styrene ND <br /> Chloroethane ND 1,1,1,2-Tetrachloroethane ND <br /> 2-Chloroethyl Vinyl Ethe ND 1,1,2,2-Tetrachloroethane ND <br /> Chloroform ND Tetrachloroethene ND <br /> ' Chloromethane ND Toluene 01ND <br /> 2-Chlorotoluene ND 1,2,3-Tnchlorobenzene ND <br /> 4-Chlorotoluene ND 1,2,4-Tnchlorobenzene ND <br /> Dlbromochlo o cthane ND 1,1,1-Trichloroethane ND <br /> ' 1,2-Dibromo-3-chloropropane ND 1,12-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene 4 0 <br /> 1,2-Dichlorobenzene ND Trichlorofluoromethane ND <br /> ' 1,3-Dichloroben2ene ND 1,2,3-Tncbloropropane ND <br /> 1,4-Dichlorobenzene ND 1,2,4-Trimethylbenzene ND <br /> Dichlorodifluoromethane ND 1,3,5-Tnmethylbenzene ND <br /> 1,1-Dichloroethane ND Vinyl Acetate"I ND <br /> ' 1,2-Dichloroethane ND Vinyl Chlonde " ND <br /> l,l-Dichloroethene ND Xylenes,total ND <br /> cis-1,2-Dichloroethene ND <br /> trans-1,2-Dichloroethene ND <br /> 1,2-Dichloropropanc ND <br /> 1,3-Dichloroprop2ne ND <br /> 2,2-Dichloropropane ND Comments <br /> 1,1-Dichloropropene ND Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND Dibromofluoromethane 100 <br /> trans-43-Dichloropropene ND Toluene-d8 104 <br /> Ethylene dibromide ND 4-Bromofluorobenzene 108 <br /> ' 'water and vapor samples are reported in ug/L,soil and sludge samples m ug/kg,wipes m ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reportmg limits unless otherwise stated water samples 10 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone,(h)lighter than water immiscible sheen is present, (1)liquid sample that contains greater than --5 vol % <br /> ' sediment,0)sample diluted due to high organic content, (k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Z1,1 Edward Hamilton,Lab Director <br />