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' 110 Second Avenue South,##D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ' hnpJwmmmccamrpbell com E-mail mam@mccampbell corn <br /> ' Advanced GeoEnvironmental Client Project ID Chase-Madison Date Sampled 11/03/98 <br /> 4005 North Wilson Way Date Received 11/06/98 <br /> ' Stockton,CA 95205 Client Contact Kevin McKibben Date Extracted 11/08/98 <br /> Client P O Date Analyzed 11/08/98 <br /> ' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 98251 <br /> ' Client ID MW-21A/11-3-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> ' Acetone NEk20 Ethylbenzene 150 <br /> Benzene 170 Hexachlorobutadiene ND<5 <br /> Bromobenzene ND<5 lodomethane ND<5 <br /> Bromochloromelhane ND<5 Isopropylbenzene 64 <br /> ' Bromodichloromethane ND<5 p4sopropyl toluene 24 <br /> Bromoform ND<5 Methyl butyl ketone` ND<5 <br /> Bromomethane ND<5 MethyleneChlonde` ND<5 <br /> n-Bucy]benzene 16 Methyl ethyl ketone' ND<5 <br /> sec-Butyl benzene 39 Methyl isobutyl ketone s' ND<5 <br /> tent-Butyl benzene NEX5 Methyl cert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND<5 Napthalene ND<5 <br /> Carbon Tetrachloride ND<5 ii-Propyl benzene 140 <br /> Chlorobenzene ND<5 Styrenes ND<5 <br /> Chloroethane ND<5 1,1,1,2-Tetrachloroethane ND<5 <br /> 2-Chloroethyl Vinyl Ether` ND<5 1,1,2,2-Tetrachloroethane ND<5 <br /> Chloroform ND<5 Tetmchlomethene 61 <br /> ' Chloromethane ND<5 Toluene W ND<5 <br /> 2-Chlorotoluene ND<5 1,2,3-Tnchlorobenzene ND<5 <br /> 4-Chlorotoluene ND<5 1,2,4-Tnchlorobenzene ND<5 <br /> Dibromochloromethane NEXS 1,1,1-Trichloroethane ND<5 <br /> 12-Dibromo-3-chloropropane ND<5 1,1,2-Tnchloroethane ND<5 <br /> Dibromomethane ND<5 Trichloroethene 21 <br /> 1,2-Dichlorobenzene ND<5 Tnchlorofluoromethane ND<5 <br /> 1,3-Dichlorobenzene ND<5 1,2,3-Tnchloropropane ND<5 <br /> 1,4-Dichlorobenzene ND<5 1,2,4-Tnmethylbenzene 250 <br /> Dichlorodi fluoromethane ND<5 1,3,5-Trimethylbenzene 58 <br /> i <br /> 1,1-Dichloroethane ND<5 Vinyl Acetate m ND<5 <br /> ' 1,2-Dichloroethane ND<5 Vinyl Chloride ° ND<5 <br /> 1,1-Dichloroethene ND<5 Xylenes,total s° 22 <br /> cis-1,2-Dichloroethene ND<5 <br /> trans-1,2-Dichloroethene ND<5 <br /> ' 1,2-Dichloropropane ND<5 <br /> 1,3-Dichloropropone ND<5 <br /> 2,2-Dchloroprop2ne ND<5 Comments h <br /> 1,l-Dichloropropene ND<5 Surrogate Recoveries <br /> cis-1,3-Dichloropropene ND<5 Dibromofluoromethane 98 <br /> trans-0-Dichloropropene ND<5 Toluene-d8 109 <br /> Ethylene dibromide IND<5 4-Bromot1uorobenzene EEJ 125 <br /> ' µater and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2 hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> ' pentanone or isopropylacetone,(h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol % <br /> sediment,O)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,0)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> i <br />