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I 10 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ' http//wwwmccampbellconi E-mail main@mccampbell com <br /> ' Advanced GeoEnviromnental Client Project ID Chase Madison Date Sampled 03/21/01 <br /> 837 Shaw Road Date Received 03/23/01 <br /> ' Stockton, CA 95215 Client Contact Paul Dotson Date Extracted 03/23/01 <br /> Client P O Date Analyzed 03123-03/27101. <br /> ' Diesel Range(C10-C23) and Oil-Range(CI 8+)Extractable Hydrocarbons as Diesel and Motor Oil* <br /> EPA methods modified 9015,and 3550 or 3514,California RWQCB(5F Bay Region)method GCFID(3550)or GCFID(3510) f <br /> Lab 1D Client 1D Matrix TPH(d)+ TPH(mo)+ %Recovery <br /> Surrogate <br /> 63682 SSW-5' S 43,g,d 100 97 <br /> ' 63683 SSN-5' S 80,9,d 190 107 <br /> 63684 TKN-5' S ND ND 105 <br /> ' 63685 TKF-9' S l l,d ND 105 <br /> ' 63686 TKW-5' S ND ND 106 <br /> 63687 TKE-5' S ND ND 106 <br /> ' • 63688 TKS-5' S ND ND 106 <br /> 63689 SSN-9' S 2100,e,g 1100 113 <br /> 63690 SSW-9' S ND ND 105 <br /> 1 <br /> Reporting Limit unless otherwise W 50 ug/L. 250 ug/L <br /> stated ND means not detected above <br /> the repoinng limit S 1 0 mg/kg 5 0 mg/kg <br /> *water samples aie reported in ug/L,wipe samples in ug/wipe,soil and sludge samples in mglkg,and all TCLP/STLC i SPLP extracts in <br /> 1 ug/L <br /> cluttered chiomatogram resulting in coeluted surrogate and sample peaks,or surrogate peak is on elevated baseline,or surrogate has been <br /> dimmislted by dilution of original extract <br /> ' `The tollowing desctiptions of the TPII chromatogram are cursory in nature and McCampbell Analyticai is not responsible for then <br /> interpretation a)unmodified of weakly modified diesel is signa,cant,b)diesel range compounds are srgtuticant no recognizable pattern,c) <br /> aged diesel' is signtiicant), d) gasoline range compounds are significant e) medium boiling point pattern that does not match diesel <br /> (stoddard solvent") t)one to a tew isolated peaks present,g)oil range compounds aie significant,h)lighter than water immiscible sheen is <br /> ' present i)liquid sampie that contains greater than—5 vol %sediment <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />