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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> 4 McCAMPBELL ANALYTICAL INC 'telephone 925-798-1620 'Fax 925-798-1622 <br /> http//www mccampbell com E-mail man@mccarnpbell com <br /> • <br /> ' Advanced GeoEnvironmental Client Project ID Chase Madison Date Sampled 11/15/00 <br /> 4005 North Wilson Way Date Received 11/17/00 <br /> Stockton, CA 95205 Client Contact Paul Dotson Date Extracted 11/17/00 <br /> Client P O Date Analyzed 11117-11/20100 <br /> Diesel Range(C10-C23)and Oil-Range(C18+)Extractable Hydrocarbons as Diesel and Motor Oil* <br /> EPA methods modified 8015,and 3550 or 3510,California RWQCB(SF Bay Region)method GCFID(3550)or GCFID(3510) <br /> Lab ID Client ID Matrix TPH(d)+ TPH(mo)+ %Recovery <br /> S urrogate <br /> 53617 15B-10-15 S 350,e ND 91 <br /> 53618 ISB-10-23 S 31,e ND 91 <br /> 53619 1513-10-32 S 99,e ND 88 <br /> 53620 15B-10-36 S 2100,e 53 105 <br /> ' 53621 15B-10-37 S ND ND 96 <br /> 53622 15B-10-40 S ND ND 93 <br /> ,• 53623 15B-11-15 S ND ND 93 <br /> 53624 1513-12-10 S 520Ac 80 93 <br /> 53625 15B-12-15 S 5700,a,d 2100 99 <br /> 53626 15B-12-20 S 920,c,d 180 91 <br /> I53627 15B-13-15 S ND ND 92 <br /> Reporting Limit unless otherwise W 50 ug/L 250 ugfL <br /> stated ND means not detected above <br /> the reporting limit S 1 0 mg/kg 5 0 mg/kg <br /> *water samples are reported in ug(L,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP/STLC/SPLP extracts in <br /> ' uglL <br /> a cluttered chromatogram resulting in coeluted surrogate and sample peaks,or,surrogate peak is on elevated baseline,or,surrogate has been <br /> diminished by dilution of original extract <br /> ' 'The following descriptions of the TPII chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation a)unmodified or weakly modified diesel is significant,b)diesel range compounds are significant,no recognizable pattern,c) <br /> aged diesely is significant),d)gasoline range compounds are significant,e)medium boiling point pattern that does not match diesel(fuel <br /> oil's),f)one to a few isolated peaks present,g)oil range compounds are significant,h)lighter than water immiscible sheen is present,i) <br /> ' liquid sample that contains greater than—5 vol %sediment <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />