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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McC.AIMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-I622 <br /> ' htta//www mccamnbell conn E-mail main@mccatnpbell com <br /> ' Advanced GeoEnvironniental Client Project ID Chase/Madison Date Sampled 02/13/2002 <br /> ' 837 Shaw Road Date Received 02/15/2002 <br /> Stockton, CA 95215 Client Contact Paul Dotson Date Extracted 02/15-02/1912002 <br /> ' Client P D Date Analyzed 02/15-02/19/2002 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> ' Lab ID 90459 90460 90461 90462 <br /> 1�IW19A/02- MW19B/02- MW20A/02- MW20B/02- Reporting Limit <br /> Client ID 13-02 13-02 13-02 13-02 <br /> ' Matrix W W W W S W <br /> Compound Concentration" ug/kg uV"L <br /> Dt-isopropyl Ether(D1PE) ND ND ND ND 5 0 10 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND ND ND 50 10 <br /> Methyl-tert Butyl Ether(MTBE) 1 8 14 ND ND 50 1 0 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 50 10 <br /> 1 ' <br /> tert-Butanol ND ND ND ND 25 50 <br /> ' Surrogate Recoveries(%) <br /> ' Dibromotluoromethane 104 98 106 102 <br /> ' Comments - <br /> *water samples are reported in ugfL,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I STLC 1 SPLP extracts in uglL <br /> ' ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)Itgbter than water immiscible sheen is present,(t)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> ' DHS Certification No 1644 Edward Hamilton, Lab Director <br /> 1 <br />