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Report Number 41460 QC Report Matrix Spike/ Matrix Spike Duplicate Date 1212012004 Project Name PARMAR TEXACO Project Number Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value its Method Analyzed Recov Recov Diff Limit Limit Benzene 41462-01 <0 50 399 396 404 418 ug/L EPA 8260B 12/15/04 101 106 416 70-130 25 Toluene 41462-01 <0 50 39 9 396 404 417 ug/L EPA 8260B 12/15/04 101 105 398 70-130 25 Tert-Butanol 41462-01 <5 0 20Q 198 189 193 ug/L EPA 8260B 12/15104 948 973 253 70-130 25 Methyl-t-Butyl Ether41462-01 <0 50 39 9 396 368 379 ug/L EPA 8260B 12/15/04 922 957 375 70-130 25 Benzene 41469-05 <0 50 406 400 404 404 ug/L EPA 82606 12/15/04 101 101 0154 70-130 25 Toluene 41469-05 <0 50 400 400 394 396 ug/L EPA 8260B 12/15/04 986 991 0 523 70-130 25 Tert-Butanol 41469-05 <5 0 200 200 186 192 ug/L EPA 8260B 12/15104 93 3 958 267 70-130 25 Methyl-t-Butyl Ether41469-05 <0 50 400 400 39 0 413 ug/L EPA 8260B 12/15/04 975 103 578 70-130 25 Benzene 41452-01 <0 50 400 400 387 382 ug/L EPA 8260B 12/14/04 967 954 132 70-130 25 Toluene 41452-01 <0 50 400 400 405 392 ug/L EPA 8260B 12/14/04 101 979 338 70-130 25 Tert-Butanol 41452-01 <5 0 200 200 198 200 ug/L EPA 8260B 12/14/04 990 998 0 791 70-130 25 Methyl-t-Butyl Ether41452-01 <0 50 400 400 35 8 354 ug/L EPA 8260B 12/14/04 894 886 0 944 70-130 25 Benzene 41460-05 <0 50 400 400 421 407 ug/L EPA 8260B 12/14/04 105 102 341 70-130 25 Toluene 41460-05 <0 50 400 400 41 8 406 ug/L EPA 8260B 12/14/04 104 101 290 70-130 25 Tert-Butanol 41460-05 <5 0 200 200 208 209 ug/L EPA 8260B 12/14104 104 104 0130 70-130 25 Methyl-t-Butyl Ether 41460-05 <0 50 400 400 399 402 ug/L EPA 8260B 12/14104 997 100 0 779 70-130 25 Approved By Jo tff KIFF ANALYTICAL, LLC 2795 2nd St, Suite 300 Davis, CA 95616 530-2974800