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Client Name Fugro West, Inc Date 12/15/1994 cme Client Acct 1810 FLAP Cert 1386 NET Job No 94 05896 Page 11 Ref Shell 880 Victor Rd , Lodi, CA/204-4416-0806 1 ' MATRIX SPIKE 1 MATRIX SPIKE DUPLICATE Matrix Matrix ' Matrix Spike Matrix Spike Spike Dup Spike Sample Spike Dup Date Run Sample Parameter k Rec k Rec RPD Amount Conc Conc Conc Units Analyzed Batch S eked ICP METALS SOLID ' Antimony (ICP) 82 8 88 1 6 2 994 NO 823 918 mg/kg dw 12/12/1994 681 223567 Arsenic (GFAA) 81 4 77 5 4 9 4 477 1 7 5 343 5 137 mg/kg 12/08/1994 464 226957 Barium (ICP} 99 5 86 1 _4 4 99 4 57 156 146 mg/kg dw 12/12/1994 684 223567 ' Beryllium (ICP) 100 1 100 4 0 3 99 4 NO 99 4 105 mg/kg dw 12/12/1994 684 223567 Cadmium (ICPI 95 6 96 4 0 3 99 4 ND 95 0 100 mg/kg dw 12/12/1994 535 223567 Chromium (ICPI 102 5 98 6 3 3 99 4 10 112 113 mg/kg dw 12/12/1994 546 223567 Cobalt (ICPI 96 0 94 8 1 3 99 4 4 a 100 104 mg/kg dw 12/12/1994 6a3 223567 ' Copper (ICP) 94 2 92 1 2 3 99 4 10 104 106 mg/kg dw 12/12/1994 428 223567 Lead (GFAA) 100 5 98 3 2 1 2 232 3 4 5 644 5 $75 mg/kg 12/08/1994 613 226957 Mercury (CVAA) 104 0 96 0 7 9 2 155 ND 2 242 2 223 mg/kg 12/15/1994 294 223233 Molybdenum (ICP) 93 9 95 5 1 7 99 4 ND 93 3 99 5 mg/kg dw 12/12/1994 482 223567 I Nickel (ICP) 96 0 92 9 3 3 99 4 12 107 108 mg/kg dw 12/12/1994 439 223567 Selenium (GFAA) 97 3 92 4 5 2 2 239 'VD 2 178 2 048 mg/kg 12/08/1.994 4G3 226957 Silver (ICP) 92 2 93 5 1 4 99 4 ^7D 91 6 97 4 mg/kg dw 12/12/1994 683 223567 T"allium (ICP) 99 3 99 9 0 6 994 ND 987 1 C40 mg/kg dw 12/12/1994 311 223567 Vanadium (ICP) 103 0 94 0 3 0 99 4 20 122 118 mg/kg aw 12/12/1994 356 223567 Zinc (ICP) 89 9 B3 1 7 9 99 4 22 111 109 mg/kg dw 12/12/1994 484 223567 TPH (Gas/BTXE Solid) 226963 ' as Gasoline 8s 0 81 0 3 3 5 00 2 7 7 1 6 75 mg/kg 12/08/1994 1553 226963 Benzene 104 8 108 7s 7 126 ND 132 137 ug/kg 12/08/1994 1553 226963 Toluene 103 4 106 3 2 8 415 ND 429 441 ug/kg 12/08/1994 1553 226963 I r NOTE Results apply only to the samples analyzed Reproduction of this report is permitted only in its entirety