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I` r „ <br /> MIMUM VERIFICATION IABORATOQNALYSIS <br /> TANK TANK TPI1-O TPH-D DTX & E CL�iIC TOTAL EDB METALS PCB <br /> # CONTENTS 8015 8015 8020 8010 LEAD LCAP/ 8270 <br /> 8.260 8260 8260 8240 7420 8240 AES or 8080 <br /> �� �I7421 AA <br /> LEADED <br /> t OAS X X :.f X X <br /> UNL OAS X X FS <br /> DIESEL X X j <br /> KEROSENE X X <br /> UNK FUEL X X X X X <br /> PROD. OIL X X <br /> CI ILOR. .a <br /> SOLVENTS X ` j!X <br /> F <br /> NONCIILOR <br /> SOLVEN'Is X X ,X <br /> WASTE~ fi <br /> ! 598 USED OIL x x xX x x <br /> All analyses methods are designated EPA methods described In EPA SW 846;1 llilyd Edition. 'Diose methods not found <br /> In SW 846, are specifically noted below. Refer to the 'SWit CB LUFt Field Manual", Appendix A-20, Table 3-5 for <br /> detection limits of motor vehicle fuels (gasoline and diesel). Refer to!•1-2-3 ",Regional Board Staff Recommendatiuns for <br /> Inlllal Evaluation and Investigation of US'1's' for the waste and motor,oil defection limits. <br /> [)election Limits That remain below lite MCI., STLC or Allowable LJuill of lite contaminant In question will he accepted, <br /> however laboratory shall ullllze the most couservallve m0hod. <br /> ; <br /> LABORATORY ANALYSES TERMINOLOOY: <br /> TPFI-O Total Petroleum Ilydrocatbon, Oasollue, OCFID (5030) 8015 mod or OC/MS 8260 <br /> TPII•D Total Petroleum Ilydtocatbou, Diesel, OC/FID (3550), 8015 mod or OC/MS 8260 <br /> BTX & E Benzene, Toluene, Xylene & Ethyl Benzene, OQPIQ 8020 or ODMS 8260 <br /> CL I IC Chlorinated Hydrocarbon, OCIIIS13 8010, OQMS 8240 <br /> TOTAL LEAD Total lead, AA 7420, AA 7421 or ICP-AES 6010 <br /> EDB Ethylene dibromide (Dl IS-AB 1803), OC/MS 8240 (DI IS-LUF1) <br /> OC-FID Oas Chromatography, Flame lonizadon Detect lon <br /> ICAP or AA Inductively Coupled Plasma Alomic Emission Spectrometry 6010 or Alonsic Absorption <br /> Spectrometry 70(1(1. Metals: Cadmium, Chrnrnluw III and VI, Lead, Zlne and Nickel. <br /> PCB Polychlorinated Blphenyls, ODMS 8270 or 80811 <br /> Method 3050 Add digestion <br /> Method 3540 Soxhlel sample preparation ;p <br /> Method 3550 Sonication sample preparation, extraction method <br /> Method 5030 Purge and ltap sample preparation <br /> QA/QC Quality Assurance/Qualily Control <br /> i <br /> Notes: To avoid false positive defection of benzene, benzene-free solvents are, to be used. Fused capillary columns are <br /> preferred to packed columns; a packed column may be used as a 'first cul" with 'dirty' samples or once the hydrocarbons <br /> have been characterized and proper QA/AC is followed. <br /> For Drinking water sources, EPA recommends that the 5(X1 series for v� latile organics be used In preference to the 600 <br /> series because the detection limits are lower and the QA/QC is better. 'JSantpl;es exhibiting any level of heavy mesal <br /> conlamInmion may require further analysis. PI IS-El ID recommends holding these samples until disposal Is Indicated. <br /> Ell23 048 (Revised 7/10/92) Page 8 <br /> I` <br />