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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCA-WBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-7984622 <br /> hJW:1/www.tnccamRhffi(;om E-mail:main@mccampbell.com <br /> W.A.Craig,Inc. Client Project ID:#3954;Mason Center Date Sampled: 11/03/00 <br /> 6940 Tremont Road Stockton Date Received: 11/03/00 <br /> Dixon,CA 95620-9603 Client Contact:Tim Cook Date Extracted: 11/03/00 <br /> Client P.O: Date Analyzed: 11/03-11/04/00 <br /> Oxygenated.Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 52123 52124 52125 52126 <br /> Reporting Limit <br /> Client ID 4A 5A 6A 4B <br /> Matrix S S S S S w <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPE) ND ND ND ND 5.0 1.0 <br /> Ethyl tert-Butyl Ether(ETRE) ND ND ND ND 5.0 1.0 <br /> Methyl-tert Butyl Ether(MTBE) ND ND ND ND 5.0 1.0 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 5.0 1.0 <br /> tert-Butanol ND ND ND ND 25 5.0 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 101 106 104 102 <br /> Comments: <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment;0)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 Z/7/ Edward Hamilton,Lab Director <br />