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110 2nd Avenue South #D7,Pacheco CA 94553-5560 <br /> [A# -McCampbcll Analytical, Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> h l/www mecum bell cam E mail maui@rnccaapbeII com <br /> Advanced GeoEnvlronmental,Inc Client Project ID Stefanos Date Sampled 01/27/04 <br /> 837 Shaw Road Date Received 01/28/04 <br /> Client Contact Donna Sexton Date Extracted 01/29/04 <br /> Stockton,CA 95215 <br /> Client P O D,1te Analyzed 01/29/04 <br /> Oxygenates and BTEX by GC/MS* <br /> Extraction Meihod.SW5030B Analytical Method SW8260B Work Order 0401328 <br /> Lab ID 0401328-OOIA 040I328-002A 0401328-003A <br /> Client ID SVEI-1200 SVFI-1400 SVEI-1600 <br /> Reporting Limit for <br /> Matrix A A A DF-1 <br /> DF 20 40 40�_..__—_------- <br /> Compound Concentration ug/kg 119 <br /> tent-Amyl methyl ether(TAME) ND<5 0 ND<10 ND<10 NA 025 <br /> Benzene ND<5 0 ND<10 ND<10 NA 0 25 <br /> t-Butyl alcohol(TBA) ND<50 ND<100 ND<100 NA 25 <br /> 1,2-Dibromoethane(EDB) ND<5 0 ND<10 ND<10 NA 0 25 <br /> 1,2-Dichloroethane(1,2-DCA) ND<5 0 ND<10 ND<10 STA 0 25 <br /> Dusapropyl ether(D1PE) ND<5 0 ND<10 ND<10 NA 0 25 <br /> Ethylbenzene 65 I 71 75 NA 025 <br /> Ethyl ten-butyl ether(ETRE) ND<5 0 ND<10 ND<10 NA 0 25 <br /> Methyl t-butyl ether(MTBE) ND<5 0 ND<10 ND<10 NA 025 <br /> Toluene 280 330 330 NA 025 <br /> Xylenes 730 770 770 NA 0 25 <br /> Surrogate Recoveries <br /> %SSI 104 1t0 102 <br /> %SS2 977 989 97 6 <br /> %SS3 955 98 2 97 <br /> Comments <br /> r water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soillsludge/solid samples inµg/kg, wipe samples inµg/wipe, <br /> product/oil/non-aqueous liquid samples in mg1L <br /> ND means not detected above the reporting limit,NIA means anaiyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,,])sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Angela Rydeltus, Lab Manager <br />