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0 0 Report Number 35108 QC Report Matrix Spike/Matrix Spike Duplicate Date 9130/2003 Project Name STEFANO'S Project Number Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Drff Parameter Sample Value Level Level Value Value Units Method Analyzed Recov Recov Diff Limit Limit Benzene 35135-20 <0 50 400 400 403 386 ug/L EPA 82606 9126103 101 96 6 423 70-130 25 Toluene 35135-20 <0 50 400 400 415 39 8 ug/L EPA 8260B 9126103 104 996 398 70-130 25 Tart-Butanol 35135-20 <5 0 200 200 197 203 ug/L EPA 8260B 9126103 984 101 297 70-130 25 Methyl-t-Butyl Ether 35135-20 10 400 400 489 480 ug/L EPA 8260B 9126103 968 946 238 70-130 25 Benzene 35074-01 <0 50 400 400 400 388 ug/L EPA 8260B 9125103 100 97 0 299 70-130 25 Toluene 35074-01 <0 50 400 400 39 3 375 ug/L EPA 8260B 9125103 98 2 938 466 70-130 25 Tert-Butanol 35074-01 <5 0 200 200 211 212 ug/L EPA 8260B 9125103 105 106 0 407 70-130 25 Methyl-t-Butyl Ether 35074-01 <0 50 400 400 422 406 ug/L EPA 8260B 9/25103 105 102 370 70-130 25 Benzene 35171-05 <0 50 400 400 39 4 398 ug/L EPA 8260B 9129103 984 995 108 70-130 25 Toluene 35171-05 <0 50 400 400 386 353 ug/l_ EPA 8260B 9129103 966 882 898 70-130 25 Tert-Butanol 35171-05 <5 0 200 200 208 211 ug/L EPA 8260E 9129103 104 106 163 70-130 25 Methyl-t-Butyl Ether 35171-05 <0 50 400 400 430 412 ug/L EPA 82606 9129103 107 103 418 70-130 25 Benzene 35108-01 <0 50 400 400 404 402 ug/L EPA 8260B 9125103 101 100 0 472 70-130 25 Toluene 35108-01 <0 50 400 400 410 402 ug/L EPA 8260B 9/25/03 102 101 187 70-130 25 Tert-Butanol 35108-01 <5 0 200 200 195 210 ug/L EPA 8260B 9125103 974 105 733 70-130 25 Methyl-t-Butyl Ether 35108-01 <0 50 400 400 418 434 ug1L EPA 82608 9125103 105 108 354 70-130 25 J i KIFF ANALYTICAL, LLC Approved By 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800