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a <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCampbell Analytical Inc 7 Telephone 925-798-1620 Fax 925-79s-1622 <br /> J/www roccampbell coin E-nmil num@niccarrilkellcom <br /> Advanced GeoEnvironmental,Inc Client Project ID Geweke Date Sampled 12/27/02 - <br /> • 837 Shaw Road Date Received 12/31/02 <br /> Stockton,CA 95215 Client Contact Bob Marty ' Date Extracted 12/31/02-01101/03 <br /> Client P O Date Analyzed 12131102-01/01/03 <br /> - Volatiles Orgamcs+Oxygenates by P&T and GUMS(Basic Target List)* t, <br /> Exh=um Method. SW5030B Analytical Method. 5W9260B Waite Older 0212473 <br /> Lab ID 0212473-OOIB <br /> Client ID May-15 <br /> Matrix Water <br /> Compound Cancentrano-;7 DF Compound Concentration • DF i <br /> Accton ND 1 0 50 tert-Am i methyl ether AME ND 10 05 <br /> Benne ND 10 05 Bromobemmne ND 1 0 05 <br /> Sromochlortm ethane ND to 05 Bromodiehloromed=e ND 10 05 <br /> Bromoform ND 10 05 Bromomethane ND to 05 <br /> 2-Butanone ElC ND 10 10 t-Butyl alcohol A ND 10 50 <br /> n-Butyl benzene ND 10 05 sec-Butyl benzene ND 1 0 05 <br /> tert-Butyl benzene ND to 05 Carbon Disulfide ND 1 0 05 <br /> Carlon Tetrachloride . ND 1 0 05 Chlorobenzene ND 10 05 <br /> Chloroethane ND 10 05 2-Chloroeth Vinyl Ether ND 10 05 <br /> Chloroform ND to 05 Chloromethane ND 10 05 <br /> 2-Chlorotoluene ND 10 05 4-Chlorotoiuene ND 10 05 <br /> Dibromochloromethane ND 10 05 1,2-Dibromo-3-cht a ND 1 0 05 <br /> 1,2-Dibromoethane EDB ND 10 05 Dibr+omomethane ND 10 05 <br /> 1,2-Dchlombenzene ND 10 05 1,3-Dchiombenzene ND 10 05 <br /> 1,4-Dichlorobenzene ND 10 05 Dichlorodifluoromethane ND 10 05 <br /> 1,1-Dichlomethane ND 10 05 1,2-Dichloroethane t,2-DCA 1 1 t 0 05 <br /> 1,1-Dichloroethene ND to 05 cis-1,2-Drchloroethene ND t 0 05 <br /> trans-1,2-Dehloroethene ND 10 05 1,2-Dichloropropane ND 10 05 <br /> 1,3-Dichlompropane ND 10 05 2,2-Dichloropropane ND 1 0 05 <br /> 1,1-Dichloro a ND 10 05 cis-1,3-Dichloroa ND 10 05 <br /> trans-l,3-Dichlom roe ND to 05 Diisopropyl ether IPE ND to 05 <br /> Eth lbenzeae ND 10 05 Ethyl tent-bu I ether ETRE ND 10 05 <br /> Hexachlorebutadiene ND 10 05 2-Hexanone ND 1 0 05 <br /> lodomethane eth !iodide ND 10 05 fsopropylbenzene ND 1 0 05 <br /> 4-1sopropyl toluene ND 10 05 Meth l-t-bu I ether TBE ND 1 0 05 <br /> Methylene chloride ND<5 5 10 05 4-Meth 1-2- tanone ID ND 1.0 05 <br /> Naphthalene ND 10 05 n-Pmpyl benzene ND t 0 05 <br /> Styrene ND 10 05 1,1,1,2-Tetrachloroethane ND 10 05 <br /> 1,1,2,2-Tetrachloroethane ND 10 05 Tetrachloroethene ND 10 05 <br /> Toluene ND 10 05 1,2,3-Tnchlorobenzene ND 10 05 <br /> 1,2,4-Tnehlorobenzene ND 10 05 1,1,1-Trichloroethane ND 10 05 <br /> 1,1,2-Trichloroethane ND to 05 Trichloroethene ND 10 05 <br /> Tnchlorofluoremethane ND 10 05 1,2,3-Trichloropropane ND 10 05 <br /> l,2,4-Tnmeth Ibenzene ND to 05 1,3,5-Tnmeth (benzene ND 10 05 <br /> Vinyl Acetate ND 10 50 Vinyl Chlonde ND 1 0 05 <br /> Xylenes ND 10 05 <br /> Surrogate Recoveries(%) <br /> %SSl 107 %SS2 985 <br /> %SS3 104 <br /> Comments <br /> water and vapor samples and all TCLP&SPLP extracts are reported in gg/L,soil/sludgetsolid samples to}µg/kg, wipe samples inµg/wipe, <br /> produrctloil/non-aqueous liquid samples in mg/L. <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted duo to high <br /> organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />