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McCampbell Analytical Inc 110 2nd A--��#D' ��,� 94553-5560 <br /> laphane 925-798-1620 Fax 925-798-1622 <br /> ri J/www bell com E-mal n corn <br /> ti Advanced GeoEnvironmental,Inc Client Project ID Geweke Date Sampled 12/27/02 <br /> 837 Shaw Road Date Received 12/31/02 <br /> Stockton,CA 95215 Client Contact- Bob Marty Date Extracted 12131/02-0I/01/03 <br /> Client P O Date Analyzed_ 12/31/02-01/01/03 <br /> Volatiles Organics+Oxygenates by P&T and GC/MS(Basic Target List)'' <br /> Extraction Method. SW5030B Analytical Mcft4 SW8260B Work Order 0212473 <br /> Lab iD 0212473-005B <br /> Client ID MW-19 <br /> Matrix Water / <br /> Compound Concentration* DF t 1i>a Comoound Concentration* DF <br /> Acetone l�RND 1 0 50 tent-Am methyl ether AME ND to 0 5 <br /> Benzene ND 1 0 O S Bromobenzeic ND 10 0 5 <br /> Bromochloromettiane ND 10 05 Bromodichloromethane ND 10 0 5 <br /> Bromoform ND 10 05 Bromomethane ND 10 0 5 <br /> 2-Butanone EK) ND 10 10 t-Bu I alcohol A ND 1 0 5 0 <br /> n-13utyl benzene ND 10 0 5 scc-BHW benzene ND 1 0 0 5 <br /> tert-But i benzene ND 10 05 Carbon Disulfide ND l 0 0 5 <br /> Carbon Tetrachloride ND 10 0 5 Chlorobenzene ND <br /> 10 0 5 <br /> Chloroethane ND 1 0 0 5 2-Chloroethyl Vin Ether ND 10 0 5 <br /> Chloroform ND 10 05 Chloromethane ND 1 0 0 5 <br /> 2-Chlorotoluenc ND 10 05 4-Chlorotoluene ND 10 N05 <br /> Dibromochloromethane ND 10 0 5 1,2-Dibromo-3-ehlo a ND 1 Q 1,2-Dibrom wane DB ND 10 05 Dibromomethane ND10 <br /> 1,2-Dichlorobenzene ND to 05 1,3-Dichlorobenzene ND 1 0 0 5 <br /> 1,4-Dichlorobenzene ND 1 0 0 5 Dichlorodifluoromethane ND l 0 0 5 <br /> 1,1-Dichlomethane ND 10 05 1,2-Dichloroedme 1,2-DCA ND 1 0 0 5 <br /> IJ-Dichloraelhene ND 10 05 cis-1,2-T?ichioroethene ND 1 0 0 5 <br /> trails-l,2-Dichloroctheae ND 10 05 42-Diehl a NO to 0 5 <br /> 1,3-Drch! ropane ND 1 0 0 5 2,2-Dichloroa ND 11% <br /> 4 5 <br /> 1,1-Drch] ,no ND to 05 CLI-1,3-Dichloroumpene ND 1 0 0 5 <br /> trans-l,3-Dichla rn a ND 10 0 S Dasa I ether TOE ND E 0 0 5 <br /> Ethylbenzene ND 1 0 0 5 Ethyl tert-butyl ether ETBE ND 10 05 <br /> Hexachlorobutadiene ND 10 0 5 2-HexanoneND i 0 0 5 <br /> 10domethane ethyl iodide ND 10 0 5 iso ro (benzene- ND 10 0 5 <br /> 4-Iso I toluene ND 1 0 0 5 Meth i-t-bu 1 ether TBE ND 10 0 5 <br /> Methylene chloride ND<5 5 ] 0 05 4-Meth i-2- tanone ®K ND 10 0 5 <br /> N hthalene ND ! 0 05 n- 1 benzene ND 1 0 0 5 <br /> Styrene ND 10 05 1,1,1,2-Tetrachloroethane ND 10 0 5 <br /> 1,1,2,2-Tetrachloroethane ND 1 0 05 Terachlorothnc ND 10Tolurne O S <br /> ND to 0 5 1,2,3-Tnchlorobenzene ND 10 0 5 <br /> 1,2,4-Tnehlorobenzene ND 10 05 1,1,1-Trichloroethane ND 1 0 0 5 <br /> 1,1,2-Tnehloroethane ND 1 0 05 Trichloroethene ND 10 0 5 <br /> Trichlorofluoromethane ND 10 05 1,2,3-Tnchloropropane ND 10 0 5 <br /> 1,2,4-Tnmeth fbenzene ND 10 0 5 1,3,5-Thmethylbenzene ND to 05 <br /> Vinyl Acetate ND 1 0 50 Vinyl Chlonde ND t 00 5 <br /> X Imes ND 1 Q 0 5 <br /> Surrogate lteeoverles(%) <br /> %SSl 105 %SS2 98 4 <br /> %SS3 101 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludge/solid samples m gg/kg, wt sam les m <br /> product/oil/non-aqueous liquid samples in mg/L P li8/w • <br /> ND means not detected above the reporting limit,N/A means analyte not applicable t0 this analysis <br /> •h)lighter than-ata immiscible sheenlpmduct is present,i)liquid sample that contains greater than-2 vol %sediment,l)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Durctor <br /> 5 <br />