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I 10 2nd Avenue South,#177,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone: 925-798-1620 Fax : 925-798-1622 <br /> httpa/www.mccampbell.com E-mail: main@mccampbel1.com <br /> • <br /> Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 01/18/00 <br /> 4005 North Wilson Way Date Received: 01/19/00 <br /> Stockton, CA 95205 Client Contact: Kevin McKibben Date Extracted: 01/21-01/24/00 <br /> Client P.O: Date Analyzed: 01/21-01/24/00 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 29316 <br /> Client ID MW-711-18-00 <br /> Matrix W <br /> Compound Concentration'" Compound Concentration' <br /> Acetone ) ND<30 trans-l,3-Dichioropropene ND <br /> Benzene ND Ethylene dibromide ND <br /> Bromobenzene ND Ethylbenzene ND <br /> Bromochioromethane ND Hexachlorobutadiene ND <br /> Bromodichloromethane ND lodomethane ND <br /> Bromoform ND lsopropy]benzene ND <br /> Bromomethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone" ND <br /> sec-Butyl benzene ND Methylene Chloride"' ND<10 <br /> tert-Butyi benzene ND Methyl ethyl ketone" ND <br /> Carbon Disulfide ND Methyl isobutyl ketone`g ND <br /> Carbon Tetrachloride ND Methyl tert-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND Naphthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Ether"' ND Styrene ND <br /> Chloroform ND 1,1,1,2-Tetrachloroethane ND <br /> Chloromethane ND 1,1,2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Teirachloroethene ND <br /> 4-Chlorotoluene ND Toluene") ND <br /> Dibromochloromethane ND 1,2,3-Trichl0robenzene ND <br /> 1,2-Dibromo-3-ch1oropropane ND 1,2,4-Trichlorobenzene ND <br /> Dibromomethane ND 1,1,1-Trichloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Trichloroethane ND <br /> 1,3-Dichlorobenzene ND Trichloroethene ND <br /> 1,4-Dichl0r0benzene ND Trichlorofluoromethane ND <br /> Dichlorodifluoromethane ND 1,2,3-Trichloropropane ND <br /> 1,1-Dichloroethane ND 1,2,4-Trimethylbenzene ND <br /> 1,2-Dichl0r0ethane ND 1,3,5-Trimethylbenzene ND <br /> 1,1-Dichloroethene ND Vinyl Acetate"" ND <br /> cis-1,2-Dichloroethene ND Vinyl Chloride 10J ND <br /> trans-1,2-Dichloroethene ND Xylenes,total 1 ND <br /> 1,2-Dichloropropane ND Comments: <br /> 1,3-Dichloropropane ND Surrogate Recoveries(U/.) <br /> 2,2-Dichloropropane ND Dibromofluoromethane 100 <br /> 1,1-Dichloropropene ND Toluene-d8 101 <br /> cis-1,3-Dichloropropene ND 4-Bromofluorobenzene 90 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples 1 ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 ug/kg;wipes 0.2ug/wipe <br /> ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br />. (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e)dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropyl acetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than --5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) metbylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethane;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />