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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone: 925-798-1620 Fax : 925-798-1622 <br /> http://www.mccampbell.com E-mail: main@mccampbell.com <br /> i <br /> Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 01/18/00 <br /> 4005 North Wilson Way Date Received: 01/19/00 <br /> Stockton,CA 95205 Client Contact: Kevin McKibben Date Extracted: 01121-01/24/00 <br /> Client P.O: Date Analyzed: 01/21-01/24/00 <br /> Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab 1D 29318 <br /> Client 1D MW-911-18-00 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetones ND<30 trans-1,3-Dichloropropene NO <br /> Benzene 1.0 Ethylene dibromide NO <br /> Bromobenzene NO Ethylbenzene 22 <br /> Bromochloromethane NO Hexachlorobutadiene NO <br /> Bromodichloromethane NO lodomethane NO <br /> Bromoforrn NO lsopropylbenzene 6.3 <br /> BTOmomethane NO p-Isopropyl toluene ND <br /> n-Bury]benzene 19 Methyl butyl ketone` NO <br /> sec-Butyl benzene 2.5 Methylene Chloride" ND<10 <br /> tert-Butyl benzene 1.2 Methyl ethyl ketone"' NO <br /> Carbon Disulfide NO Methyl isobutyl ketone x ND <br /> Carbon Tetrachloride NO Methyl tert-Butyl Ether(MTBE) --- <br />. Chlorobenzene NO Naphthalene ND <br /> Chloroethane NO n-Propyl benzene 10 <br /> 2-Chloroethyl Vinyl Ether" NO Styrene NO <br /> Chloroform NO 1,1,1,2-Tetr3chloroethane NO <br /> Chloromethane NO 1,1,2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND <br /> 4-Chlorotoluene ND Toluene"I ND <br /> Dibromochloromethane ND 1,2,3-Trichlorobenzene NO <br /> 1,2-Dibromo-3-chloropropane ND 1,2,4-Trichlorobenzene NO <br /> Dibromomethane NO 1,1,1-Trichloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Trichloroethane NO <br /> 1,3-Dichlorobenzene NO Trichloroethene NO <br /> 1,4-Dichlorobenzene ND Trichlorofluoromethane NO <br /> Dichlorodifluoromethane ND 1,2,3-Trichloropr0p2ne ND <br /> ),I-Dichloroethane ND 1,2,4-Trimethylbenzene 37 <br /> 1,2-Dichloroethane 25 1,3,5-Trimethylbenzene 5.6 <br /> 1,1-Dichloroethene NO Vinyl Acetate "' 3.5 <br /> cis-1,2-Dichloroethene NO Vinyl Chloride`°' NO <br /> trans-1,2-Dichloroethene NO Xylenes,total ` 6.2 <br /> 1,2-Dichloropropane ND Comments: <br /> 1,3-Dichloropropane NO Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND Dibromofluoromethane 99 <br /> 1,1-Dichloropropene NO Toluene d8 94 <br /> cis-1,3-Dichloropropene NO 4-Bromofluorobenzene 84 <br /> .water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug(L <br /> Reporting limits unless otherwise stated:water samples 1 ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 ug/kg;wipes 0.2uglwipe <br /> NO means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chlorocthoxy)ethene; (d) 2-hexanone; (e)dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i)liquid sample that contains greater than —5 vol. % <br /> sediment; 6) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />