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110 Second Avenue South,##D7,Pacheco,CA 94553-5560 <br /> MCCAWBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> htW. www mccam»bell.com E-mail rnatn@mccarnpbell com <br /> Date Sampled 09/11/98 <br /> Advanced GeoEnvironmental Client Project ID Cherokee Truck Stop <br /> Date Received 09/15/98 <br /> 4005 North Wilson Way <br /> Stockton,CA 95205 Client Contact Kevin McKibben Date Extracted 09/15-09/16198 <br /> [Client P 0 Date Analyzed 09115-09116/98 <br /> Volatile Organics By GCIMS <br /> EPA method 8260 <br /> Lab ID 95041 <br /> Client ID UST3/9-11-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND Ethylbenzene ND <br /> Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND Isopropylbenzene ND <br /> Bromodichloromethane ND p-Isopropyl toluene ND <br /> Bromoform NO Methyl butyl ketone ND <br /> Bromomeflwc ND Methylene Chloride") ND <br /> n-Butyl benzene ND Methyl ethyl ketone ND <br /> sec-Butyl benzene ND Metbyl isobutyl ketone ND <br /> tent-Buty]benzene ND Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND Naphthalene ND<10 <br /> Carbon Tetrachlonde ND n-Propyl benzene ND <br /> Chlombenzene ND Styrene ND <br /> Chloroethane ND 1,1,1,2-Tetrachloroethane ND <br /> 2-Chloroethyl Vinyl Ether" ND 1,1,2,2-Tetrachloroethane ND <br /> Chloroform ND Tetrachloroethene ND <br /> Chloromethane ND Toluene ND <br /> 2-Chlorotoluene ND 1,2,3-Tnchlorobenzene ND <br /> 4-Chlorotoluene ND 1,2,4-Tnchlorobenzene ND <br /> Dibromochioromethane ND 1,1,1-Tnchloroethane ND <br /> 1,2-Dibromo-3-chloropropane ND 1,12-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br /> 1,2-Dichlorobenzene ND Tnchlorofluoromethane ND <br /> I� I,3-Dichlorobenzene ND 1,2,3-Trichloropropane ND <br /> 1,4-Dichlorobenzene ND 1,2,4-Tnmethylbenzene ND <br /> Dichlorodifluoromethane ND 1,3,5-Tnmethylbenzene ND <br /> 1,1-Dichloroethane ND Vinyl Acetate ND <br /> 1,2-Dichloroethane ND Vinyl Chloride ° ND <br /> I,1-Dichloroethene ND Xylenes,total ND <br /> cis-1,2-Dichloroethene ND <br /> trans-1,2-Dichloroethene ND <br /> 1,2-Dichloropropane ND <br /> 1,3-Dichloropropane ND <br /> 2,2-Dichloropropane ND Comments <br /> 1,1-Dichloropropene I ND I Surrogate Recoveries(%) <br /> cis-1,3-Diehloropropene ND Dibromofluoromethane 103 <br /> trans-l,3-Dichloropropene ND Toluene-d8 104 <br /> Ethylene dibromide ND 4-13romofluorobenzene 109 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 10 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2 propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2 butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (t)liquid sample that contains greater than —5 vol % <br /> sediment,(1)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,0)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 //t Edward Hamilton,Lab Director <br />