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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> E-mail mam@mccampbell cam <br /> Date Sampled 09/11/98 <br /> Advanced GeoEnvironmental Client Project ID Cherokee Truck Stop <br /> Date Received 09/15/98 <br /> 4005 North Wilson Way <br /> Stockton,CA 95205 Client Contact Kevin McKibben Date Extracted 09/15-09/16/98 <br /> Client P O Date Analyzed 09/15-09/16/98 <br /> Volatile Organics By GC/MS <br /> EPA method$260 <br /> Lab ID 95043 <br /> Client ID USTS/9-11-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone NIX5 Ethylbenzene ND<5 <br /> Benzene 2 4 Hexachlorobutadiene ND<5 <br /> Bromobenzene ND<5 lodomethane ND<5 <br /> Bromochloromethane ND<5 Isopropylbenzene ND<5 <br /> Bromodiehloromethane ND<5 p-Isopropyl toluene ND<5 <br /> Bromoform ND<5 Methyl butyl ketone NIX5 <br /> Bromomethane ND<S Methylene Chlonde` ND<5 <br /> n-Butyl benzene NIX5 Methyl ethyl ketone ND<5 <br /> sec-Butyl benzene ND<5 Methyl isobutyl ketone Is ND<5 <br /> tert-Butyl benzene NIX5 Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND<5 Naphthalene ND<20 <br /> Carbon Tetrachloride ND<5 n-Propyl benzene ND<5 <br /> Chlorobenzene ND<5 Styrene WND<5 <br /> Chloroethane ND<5 1,1,1,2-Tetrachloroethane ND<5 <br /> 2-Chloroethyl Vinyl Eth ` ND<5 1,1,2,2-Tetrachloroethane ND<5 <br /> J Chloroform ND<5 Tetrachloroethene ND<5 <br /> Chloromethane NIX5 Toluene ND<5 <br /> 2-Chlorotoluene ND<5 1,2,3-Tnchlorobenzene ND<5 <br /> 4-Chlorotoluene ND<5 1,2,4-Tnchlorobenzene ND<5 <br /> Dibromochloromethane ND<5 1,1,1-Tnchloroethane ND<5 <br /> 1,2-Dibnomo-3-chloropropane ND<5 1,1,2-Tnchloroethane ND<5 <br /> Dibromomethane ND<5 Trichloroethene ND<5 <br /> 1,2-Dichlorobenzene ND<5 Tnchloroflueromethane ND<5 <br /> 1,3-Dichlorobenzene ND<5 1,2,3-Tnchloropropane ND<5 <br /> 1,4-Dichlorobenzene ND<5 1,2,4-Tnmethylbenzene ND<5 <br /> Dichlorodifluoromethane ND<5 1,3,5-Tnmethylbenzene ND<5 <br /> 1,1-Dichloroethane ND<5 Vinyl Acetate °, 60 <br /> 1,2-Dichloroethane 580 Vinyl Chloride ° ND<5 <br /> 1,1-Dichloroethene ND<5 Xylenes,total ND<5 <br /> cis-1,2-Dichloroethene ND<5 <br /> trans-l,2-Dichloroethene ND<5 <br /> 1,2-Dichloropropane ND<5 <br /> 1,3-Dichloropropane ND<5 <br /> 2,2-Dichloropropane ND<5 Comments <br /> 1,1-Dichloropropene NIX5 Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND<5 Dibromofluoromethane 102 <br /> trans-l,3-Dichloropropene ND<5 Toluene-d8 164 <br /> Ethylene dibroirude ND<5 4-Bromotluorobenzene 47 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 10 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5 uglkg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-bexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than—5 vol % <br /> sediment,G)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,0}tnethylbenzene,(m)acetic acid ethenyl ester,(n)chlomethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />