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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> Ih //www mccMn bell com E-mail matn@mccampbell com <br /> Advanced GeoEnvironmental Client Project M Cherokee Truck Date Sampled 09/20/2000 <br /> 4005 North Wilson Way Date Received 09/21/2000 <br /> Stockton, CA 95205 Client Contact Tony Mikacich Date Extracted 09/22/2000 <br /> Client P O Date Analyzed 09/22/2000 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 48130 <br /> Client ID Large Well-09120/00 <br /> Matrix W <br /> Compound Concentration* Rcp°rtmgL¢mt Compound Concentration* Reporting Limit <br /> W S W I S <br /> Acetone i ND 5 0 25 trans-1,3-Dichloropropene ND 1 0 5 0 <br /> Benzene ND 10 5 0 Ethylene dibromide ND 1 0 5 0 <br /> Bromobenzene ND 10 5 0 Ethylbenzene ND 1 0 5 0 <br /> Bromochloromethane ND 10 5 0 14exachiorobutadiene ND 5 0 25 <br /> Bromodichloromethane ND 10 50 Iodomethane ND 1 0 50 <br /> Bromoform ND 10 5 0 isopropyibenzene ND 10 50 <br />' Bromomethane ND 10 50 p-Isopropyl toluene ND to 5 0 <br /> n-Butyl benzene ND 10 50 Methyl butyl ketone ND 10 5 0 <br /> sec-Butyl benzene ND 10 50 Methylene Chloride(e) ND<5 0 10 5 0 <br /> tert-Butyl benzene ND 10 5 0 Methyl ethyl ketone ND 2 0 10 <br /> Carbon Disulfide ND l 0 50 Methyl isobutyl ketone a ND 10 5 0 <br /> Carbon Tetrachloride ND 1 0 5 0 Methyl tert-Butyl Ether(MTDE) --- 10 5 0 <br /> Chlorobenzene ND 1 0 5 0 Naphthalene ND 50 5 0 <br /> 1 <br /> Chloroethane ND 10 5 0 n-Propyi benzene ND 10 5 0 <br />' 2-Chloroethyl Vinyl Ether"' ND 1 0 5 0 Styrene ND 10 5 0 <br /> Chloroform ND 1 0 50 1,1,1,2-Tetrachloroethane ND 10 5 0 <br /> Chloromethane ND 10 5 0 1,1,2,2-Tetrachloroethane ND 1 0 5 0 <br /> 2-Chlorotoluene ND 1 0 5 0 Tetrachloroethene ND 10 5 0 <br />' 4-Chlorotoluene ND 10 50 Toluene ND 10 50 <br /> Dibromocbloromethane ND 1 0 50 1,2,3-Tnchloroberizene ND 5 0 25 <br /> 1,2-Dibromo-3-chloropropane ND 20 10 1,2,4-Tnchlorobenzene ND 50 25 <br /> Dibromomethane ND 10 5 0 1,1,1-Tnehloroethane ND 10 5 0 <br />' 1,2-Dichlorobenzene ND 10 5 0 1,1,2-Trichloroethane ND 10 50 <br /> 1,3-Dichlorobenzene ND 10 5 0 1 Tnchloroethene ND 1 0 5 0 <br /> 1,4-Dichlorobenzene NO 10 5 0 Trichlorofluoromethane ND 1 0 5 0 <br /> Dichlorodifluoromethane ND to 50 1,2,3-Tnchloropropane ND 1 0 5 0 <br />' 1,1-Dichloroethane ND 10 5 0 1,2,4-Trimethylbenzene ND 1 0 5 0 <br /> 1,2-Dichloroethane ND 10 5 0 1,3,5-Tnmethylbenzene ND 10 50 <br /> 1,1-Dichloroethene ND 1 0 50 Vinyl Acetate `° ND 50 25 <br /> cis-1,2-Dichloroethene ND 1 0 5 0 Vinyl Chloride " ND 1 0 50 <br />' trans-1,2-Diehloroethene ND 10 5 0 Xylenes,total ND 1 0 50 <br /> 1,2-Dichicropropane ND 10 5 0 Comments <br /> 1,3-Dichlornpropane ND 10 5 0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 10 5 0 Dibromofluoromethane 103 <br />' <br /> 1,1-Dichloropropene ND 10 50 Toluene-d8 100 <br /> cis-1,3-Dichloropropene ND 10 50 4-Bromofluorobenzene 95 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy)ethene, (d)2-hexanone (e)dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or tsopropylacetone, (h)lighter than water immiscible sheen is present, (1)liquid sample that contains greater than--5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzen (1) methylbenzene, (m) acetic acid ethenyl ester (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> 1 <br />