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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' h //www WpgMphell,corri E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Cherokee Trucking Date Sampled 09/28-09/29/00 <br /> 4005 North Wilson Way Date Received 10/02/00 <br />' Stockton,CA 95205 Client Contact Tony Mikacich Date Extracted 10/04-10/05/00 <br />' Client P O Date Analyzed 10104-10/05100 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 49052 <br /> Client ID UST-2109-28-00 <br /> Matrix W <br /> Compound Concentration* Repumng Limit Compound Concentration* Reporting <br /> Limit <br />' W 5 I W S <br /> Acetone ND<10 50 25 trans-1,3-Dichloropropene ND to 50 <br /> Benzene ND 1 0 50 Ethylene dibromide ND 10 5 0 <br /> Bromobenzene ND 1 0 50 Ethylbenzene ND 10 5 0 <br />' Bromochloromethane ND 10 5 0 14exachlowbutadiene ND 50 25 <br /> Bromodichloromethane ND 10 50 todometbane ND 10 50 <br /> Bromoform ND 1 0 5 0 Isopropylbenzene ND to 5 0 <br /> Bromomethane ND 1 0 50 p-Isopropyl toluene ND 10 5 0 <br />' n-Butyl benzene ND 1 0 5 0 Methyl butyl ketone ND 10 5 0 <br /> sec-Butyl benzene ND 1 0 50 Methyiene Chlonde` NDc5 10 5 0 <br /> tert-Butyl benzene ND 10 5 0 Methyl ethyl ketone ND 2 0 10 <br /> Carbon Disulfide ND to 5 0 Methyl isobutyl ketone ND 10 50 <br /> Carbon Tetrachloride ND 1 0 50 Methyl tert-Butyl Ether(MTBE) - 10 5 0 <br /> Chlorobenzene ND 10 5 0 Naphthalene ND 50 50 <br /> Chloroethane ND 10 5 0 n-Propyl benzene ND 10 5 0 <br />' 2-Chlomethyl Vinyl Ethe ° ND 11 5 0 Styrene ND 10 50 <br /> Chloroform ND 1 0 5 0 1,1,1,2-Tetrachloroethane ND 10 50 <br /> Chloromethane ND 10 50 1,1,2,2-Tetrachloroethane ND 10 50 <br /> 2-Chlorotoluene ND 1 0 5 0 Tetrachloroethene ND<5 10 50 <br />' 4-Chlorotoluene ND 1 0 5 0 Toluene 11 ND 10 5 0 <br /> Dibroniochloromethane ND 10 50 12,3-Tnchlorobenzene ND 50 25 <br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnchlorobenzene ND 5 0 25 <br /> Dibromoinethane ND 10 50 1,1,1-Tnchloroethane ND 10 50 <br />' 1,2-Dichlorobenzene ND 10 5 0 1,1,2-Trichloroethane ND 10 50 <br /> 1,3-Dichlorobenzene ND 1 0 50 Crichlorocthene ND 10 5 0 <br /> 1,4-Dichlorobenzene ND 1 0 50 Tnchlorofluoromethane ND 10 5 0 <br /> Dichlorodifluoromethane ND 10 50 1,2,3-Tnchloropropane ND 10 5 0 <br />' 1,1-Dichloroethane ND 1 0 50 1,2,4-Tnmethylbenzene ND 10 50 <br /> 1,2-Dichloroethane ND 10 50 1,3,5-Tnmethylbenzene ND 10 5 0 <br /> 1,1-Dichloroethene ND to 50 Vinyl Acetate m ND 5 0 25 <br /> cis-1,2-Dichloroethene ND to 50 Vinyl Chloride ND 10 5 0 <br />' trans-1,2-Dichloroethene ND to 5 0 Xylenes,total ND 10 50 <br /> 1,2-Dichloropropane ND to 50 Comments <br /> 1,3-Dichloropropane ND 10 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 10 50 Dibromotluoromethane 109 <br />' 1,1-Dichloropropene ND L 0 50 Toluene-d8 99 <br /> cis-1,3-Dichloropropene ND 10 50 4-Bromofluorobenzene 78 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2thloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isapropylacetonc, (h)lighter than water i—sc,ble sheen is present, (i)liquid sample that contains greater than –5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene (m) acetic acid ethenyl ester (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />