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I <br /> 110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 ' <br /> hM2,//www mccampbell corn E-mail main@mccampbell corn <br /> Advanced GeoEnvironmental Client Project ID Cherokee Trucking Date Sampled 09/28-09/29/00 <br /> 4005 North Wilson Way Date Received 10/02/00 <br />' Stockton, CA 95205 Client Contact Tony Mikacich Date Extracted 10104-10/05100 <br />' Client P O Date Analyzed 10/04-10/05/00 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 49055 <br /> Client ID UST-5/09-28-00 <br /> Matrix W <br /> Reporting Limn Reporting Ltmn <br />' Compound Concentration* W S Compound Concentration* W S <br /> Aectone ND<130 50 25 trans-1,3-Dichloropropene ND<i0 10 50 <br /> Benzene 12 1 0 50 Ethylene dibromide ND<10 10 50 <br />' Bromoberizene ND<10 10 50 Ethylbenzene ND<10 10 50 <br /> Bromochloromethane ND<10 1 0 50 Hexachlorobutadiene ND<10 50 25 <br /> Bromodichloromethane ND<10 10 50 Iodomethane ND<IO 10 50 <br /> Bromoform ND<10 1 0 50 Isopropylbenzene ND<10 10 so <br /> Bromomethane ND<10 10 50 p-Isopropyl toluene ND<10 10 50 <br /> I n-Butyl benzene ND<10 1 0 50 Methyl butyl ketone ND<10 10 50 <br /> sec-Butyl benzene ND<10 1 0 50 Methylene Chlonde` ND<25 10 50 <br /> tent-Butyl benzene ND<10 1 0 50 Methyl ethyl ketone ND<10 20 10 <br /> Carbon Disulfide ND<10 1 0 50 Methyl isobutyl ketone ND<10 10 50 <br /> Carbon Tctrachlonde ND<10 1 0 50 Methyl tent-Butyl Ether(MTBE) -- 10 50 <br /> Chlorobenzene ND<10 1 0 50 Naphthalene ND<10 50 50 <br /> Chloroethane ND<10 1 0 50 n-Propyl benzene ND<10 10 50 <br />' 2-Chloroethyl Vinyl Ether') ND<10 1 0 50 Styrene ND<10 10 50 <br /> Chloroform ND<10 1 0 50 1,1,1,2-Tetrachloroethane ND<10 10 so <br /> Chloromethane ND<10 1 0 50 1,1,2,2-Tetrachloroethane ND<10 10 50 <br /> 2-Chlorotoluene ND<10 10 50 Tetrachloroethene ND<10 10 50 <br /> 4-Chlorotoluene ND<10 1 0 50 Toluene ND<10 lo 50 <br /> Dibromochloromethane ND<10 to 50 1,2,3-Tnchlorobenzene ND<10 so 25 <br /> 1,2-Dibromo-3-chloropropane ND<10 20 10 1,2,4-Tnchlorobenzene ND<10 so 25 <br /> Dibromomethane ND<10 to 50 1,1,1-Tnchloroethane ND<10 10 50 <br />' 1,2-Dichlorobenzene ND<10 10 50 1,12-Trichloroethane ND<10 10 50 <br /> 1,3-Dichlorobenzene ND<10 1 0 50 Tnchloroethene ND<10 10 so <br /> 1,4-Dichlorobenzene ND<10 1 0 50 Trichlorofluoromethane ND<10 10 so <br /> Dichlorodifluoromethane ND<10 10 50 1,2,3-Trichloropropane ND<IO 10 50 <br />' l,l-Dichloroethane ND<10 10 50 1,2,4-Tnmethylbenzene ND<10 10 50 <br /> 1,2-Dichloroethane 750 1 0 50 1,3,5-Tnmethylbenzene ND<10 10 50 <br /> 1,1-Dichloroethene ND<10 10 50 Vinyl Acetate m Np<10 50 25 <br /> cis-1 2-Dichloroethene ND<10 10 50 Vinyl Chlonde ND<10 10 50 <br />' trans-1,2-Dichloroethene ND<10 10 50 Xylenes,total NiX10 10 50 <br /> 1,2-Dichloropropane NiXIO 10 50 Comments <br /> 1,3-Dichloropropane ND<10 10 50 Surrogate Recoveries(%) <br /> 2,2-13ichloropropane ND<10 1 0 5 0 Dibromofluoromethane 119 <br />' 1,1-Dichloropropene ND<10 1 0 50 Toluene-d8 99 <br /> cis-1,3-Dichloropropene ND<10 1 0 50 4-13romofluorobenzene 71 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chlormthoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (t} 2-butanone, (g) 4-methyl-2- <br /> pentanone or i,opropylacolone, (h)lighter than water immiscible sheen Ls present, (i)liquid sample that contains greater than —5 vol % <br /> sediment, (1) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> I <br />