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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br />' w McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h //WMM mccampbell corn E-mail main@mecampbell corn <br /> Advanced GeoEnvironmental Client Project ID Cherokee Trucking Date Sampled 06/14/00 <br /> 4005 North Wilson Way Date Received 06/15/00 <br /> 1 Stockton, CA 95205 Client Contact Tony Mlkacich Date Extracted 06/16-06/19/00 <br />' Client P O Date Analyzed 06116-06/19/00 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 40404 <br /> Client ID UST-4/06-14-00 <br /> Matrix W <br /> * Repomng Lima Reporting unlit <br />' Compound Concentration* W S Compound Concentration* <br /> W S <br /> Acetone<e) NO 50 25 trans-l,3-Dichloropropene NO 10 50 <br /> Benzene NO 10 50 Ethylene dibronude NO 10 50 <br />' Bromobenzene NO 10 50 Ethylbenzene NO 10 50 <br /> Bromochloromethane NO 10 50 Hexachlorobutadiene NO 50 25 <br /> Bromodtchloromethane NO 1 0 50 Iodomethane NO 1 0 50 <br /> Bromoform NO 10 50 Isopropylbenzene ND 10 50 <br />' Bromomethane NO 10 50 p-Isopropyl toluene ND 10 50 <br /> n-Butyl benzene ND 10 50 Methyl butyl ketone NO 10 50 <br /> sec-Butyl benzene NO 10 50 Methylene Chloride(') NO 1 0 50 <br /> tent-Butyl benzene NO 10 50 Methyl ethyl ketone ND 20 10 <br /> Carbon Disulfide NO to 50 Methyl isobutyl ketone a NO 10 50 <br /> Carbon Tetrachloride ND 10 50 Methyl tent-Butyl Ether(MTBE) to 50 <br /> Chlorobenzene NO 10 50 Naphthalene NO 50 50 <br /> Chloroethane NO 10 50 n-Propyl benzene NO 10 50 <br /> I 2-Chloroethyl Vinyl Ether ) NO 10 50 Styrene NO 1 0 50 <br /> Chloroform ND 10 50 1,1,1,2-Tetrachloroethane NO —T—o 50 <br /> Chloromethane NO 10 50 1,1,2,2-Tetrachloroethane NO 10 50 <br /> 2-Chlorotoluene ND 10 50 Tetrachloroethene ND<2 0 10 50 <br /> I 4-Chlorotoluene NO 1 0 50 Toluene NO 1 0 50 <br /> Dibromochloromethane NO 10 50 1,2,3-Tnchlorobenzene NO 50 25 <br /> 1,2-Dibromo-3-chloropropane NO 20 10 1,2,4-Tnchlorobenzene NO 50 25 <br /> Dibromomethane NO 10 50 1,1,1-Tnebloroethene ND 10 50 <br /> 1,2-Dichlorobenzene NO 10 50 1,1,2-Trichloroethane ND 10 50 <br /> 1,3-Dichlorobenzene NO 1 0 50 Trichloroethene ND 10 50 <br /> 1,4-Dichlorobenzene NO 10 50 Tnchlorofluoromethane NO 1 0 <br /> so <br /> Dichlorodifluoromethane NO 10pso <br /> 1,2,3-Tnchloropropane ND 10 50 <br /> 1,1-Dichloroethane NO 10 1,2,4-Trimethylbenzene NO 10 50 <br /> 1,2-Dichloroethane NO 10 1,3,5-Tnmethylbenzene ND 10 50 <br /> t,1-Dichloroethene NO 1 0 Vinyl Acetate °' NOU10 <br /> 25 <br /> cis-1,2-Dichloroethene ND 10 Vinyl Chloride ° NO so <br /> I trans-1,2-Dichloroethene NO 1 6 Xylenes,total ND5 0 <br /> 1,2-Dichloropropane NO 10 50 Comments <br /> 1,3-Dichloropropane NO to 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane NO 10 50 Dibromofluoromethane 124 <br /> 1,1-Dichloropropene NO 1 0 50 Toluene-d8 101 <br /> cis-1,3-Dichloropropene NO 10 50 1 4-Bromofluorobenzene 82 <br /> `water and vapor samples are reported in ug/L,soil and sludge samples in ugIkg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> NO means not detected above the reporting limit,N/A means analyte not appltcable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane, (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacelone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 i Edward Hamilton,Lab Director <br />