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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAWBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> i 24 htto J vww.mccampbell coin E-mail main@mccampbell coin <br /> Advanced GeoEnvironmental Client Protect ID Cherokee Truck Stop Date Sampled 09/23/99 <br /> 4005 North Wilson Way Date Received 09/25/99 <br />' Stockton,CA 95205 Client Contact Kevin McKibben Date Extracted 09/27-09/30/99 <br />' Client P O Date Analyzed 09/27-09/30/99 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 22095 <br /> Client ID UST4/9-23-99 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone m' ND trans-1,3-Dichloropropene ND <br /> Benzene ND Ethyiene dibromide ND <br /> Bromobenzene ND Ethylbenzene ND <br /> Bromochloromethane ND Hexachlorobutadiene ND <br />' Bromodichloromethane ND lodomethane ND <br /> Bramoform ND lsopropylbenzene ND <br /> Bromomethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketoneND <br /> sec-Butyl benzene ND Methylene Chloride" NDS <br /> tert-Butyl benzene ND Methyl ethyl ketone ND <br /> Carbon Disulfide ND Methyl isobutyl ketone a ND <br /> Carbon Tetrachlonde ND Methyl tert-Butyl Ether(MTBE) --- <br />' Chlorobenzene ND Naphthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Ether" ND Styrene M ND <br />' Chloroform ND 1,1,1,2-Tetrachloroethane ND <br /> Chloromethane ND 1,1,2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND <br /> 4-Chlorotoluene ND Toluene'"' ND <br /> Dibromochloromethane ND 1,2,3-Tnchlorobenzene ND <br /> 1,2-Dibromo-3-chloropropane ND 1,2,4-Tnchlorobenzene ND <br /> Dibromomethane ND 1,1,1-Tnchloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Trichloroethane ND <br />' 1,3-Dichlorobenzene ND Tnchloroethene ND <br /> 1,4-Dich10robenzene ND Tnchlorofluoromethane ND <br /> Dichlorodifluoromethane ND 1,2,3-Tnchloropropane ND <br /> 1,1-Dichloroethane ND 1,2,4-Tnmethylbenzene ND <br />' 1,2-Dichloroethane ND 1,3,5-Tnmethylbenzcne ND <br /> 1,1-Dichloroethene ND Vinyl Acetate'" ND <br /> cis-1,2-Dichloroethene ND Vinyl Chloride" ND <br /> trans-1,2-Dichloroethene ND Xylenes,total 'PI ND <br /> 1,2-Dichloropropane ND Comments <br /> 1,3-Dichloropropane ND Surrogate Reco-tcries(%) <br /> 2,2-Dichloropropane ND Dibromofluoromethane 102 <br /> IJ-Dichloropropene ND Toluene-dg 97 <br /> cis-1,3-Dichloropropene ND 4-Bromofluorobenzene 117 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/ttiipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated eater samples 1 ug/L,%apor samples 0 5 ug/l-,solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> . (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone (e) dichloromethane, (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present (i) liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> L.Shloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644Edward Hamilton,Lab Director <br />