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1 <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' http llwww mccampbell com E-mail main@mccampbell com <br /> i <br />' Advanced GeoEnvironmental Client Protect ID Cherokee Truck Stop Date Sampled 09/27-09/29/99 <br /> 4005 North Wilson Way Date Received 10/01/99 <br />' Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 10/01/99 <br /> Client P O Date Analyzed 10/01-10/04/99 <br /> Oxygenated Volatile Organics By GC/FIS <br /> EPA method 8260 modified <br />' Lab ID 22523 22530 22539 22546 <br /> Reporting Limit <br /> Client ID B18-20 B20-5 B22-35 B25-30 <br /> Matrix S S S S S w <br /> Compound Concentration* ug/kg ug/L <br />' Di-isopropyl Ether(DIPE) ND ND ND ND 50 10 <br />' Ethyl tert-Butyl Ether(ETBE) ND ND ND ND 50 10 <br /> Methyl-tert Butyl Ether(MTBE) ND 5 7 ND ND so 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 50 1 0 <br />' tert-Butanol ND ND ND ND 25 50 <br />' Surrogate Recoveries(%) <br />' Dibromofluoromethane 104 100 100 93 <br /> Comments <br />' *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br />' (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> I <br />