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110 2nd Avenue South,#D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925-798-1620 Fax 925 798-1622 <br /> ho Website www mccampbell com F-mail main@mccampbell corn <br />' Advanced GeoEnvironmental, Inc Client Project ID Cherokee Truck Stop Date Sampled 06/03/04 <br /> 837 Shaw Road Date Received 06/04/04 <br /> Client Contact Paul Dotson Date Extracted 06105/04-06/07/04 <br />' Stockton,CA 95215 Client P O Date Analyzed 06/05/04-06/07/04 <br /> Volatiles Organics by P&T and GUMS(Bask Target List)* <br />' Extraction Method Analytical Method SW8260B Work Order 0406066 <br /> Lab ID 0406066-003B <br /> Client ID UST-4 <br />' Matrix Water <br /> Compound Concentration* DF x` n g Compound Concentration* DF R`L-„ <br /> Acetone ND to 50 Acrolem(Propenal) ND 1 0 50 <br />' <br /> Acrylonitrale ND to 20 tert-Amyl methyl ether AME ND 1 0 05 <br /> Benzene ND to 0 5 Bromobcnzene ND 1 0 o5 <br /> Bromochloromethane ND to 0 5 Bromodichloromethane ND 1 0 05 <br /> Bromoform ND 10 05 Bromomethane ND 1 0 05 <br />' 2-Butanone(MEK) ND 10 10 t-But 1 alcohol(TBA) ND 1 0 50 <br /> n-But 1 benzene ND 1 0 05 sec-Butyl benzene ND 1 0 05 <br /> tert-But 1 benzene ND 10 05 Carbon Disulfide ND 1 0 05 <br /> Carbon Tetrachloride ND 10 hiorobenzene ND 1 0 05 <br />' Chloroethane ND 10 05 1 2 Chloroeth 1 Vinyl Ether ND 10 1 0 <br /> Chloroform ND 10 05 Chloromethane ND 1 0 05 <br /> 2-Chlorotoluene ND 10 05 4-Chlorotoluene ND 1 0 05 <br /> Dibromochloromethane ND 10 05 1,2-Dibromo-3-chloropro ane ND 1 0 05 <br />' 1,2-Dibromoethane(ED13) ND 10 05 Dibromomethane ND 1 0 05 <br /> 112-Dichlorobenzene ND 10 05 1,3-Dichlorobenzene ND 1 0 0 5 <br /> 1,4-Dichlorobenzene ND 10 05 Dichlorodifluoromethane ND 1 0 05 <br /> 1,1-Dichloroethane ND 10 05 1,2-Dichloroethane 1,2-DCA) ND 1 0 05 <br />' 1,1-13ichloroethene ND 1 0 0 5 cis-1,2-Dichloroethene ND 1 0 05 <br /> trans-1,2-Dichloroethene ND 10 0 5 1,2-Dtchloro ro ane ND 1 0 o5 <br /> 13-Dtchloro ro ane ND 10 0 5 2 2-Dichloro ro ane ND 1 0 05 <br />' 1 1-Dichlororopene ND 1.0-.-- 05 cis-1,3-Dichloro roene ND 1 0 05 <br /> trans-1 3-Dichloro ropene ND 1 0 0 5 Diisoprop t ether(DIP1 ND 1 0 05 <br /> Eth !benzene ND 10 05 Ethyl tert-but 1 ether ETBE ND 1 0 05 <br /> Hexachlorobutadiene ND 10 05 Hexachloroethane ND I O 05 <br />' 2-Hexanone ND 10 0 5 Isopropylbenzene ND 1 0 0 5 <br /> 4-Isopropyl toluene ND 10 05 Meth l-t-buty]ether MTBE ND 1 0 0 5 <br /> Methylene chloride ND 10 05 4-Meth 1-2- entanone(MIRK) ND 10 05 <br /> Naphthalene ND 10 0 5 Nitrobenzene ND I D t0 <br />' n-Propyl benzene ND 10 0 5 Styrene ND 1 0 05 <br /> 1,1,1,2-Tetrachloroethane ND 1 10 05 1,1,2,2-Tetrachloroethane ND 1 0 05 <br /> Tetrachloroethene ND 10 0 5 Toluene ND 1 0 1 0 5 <br /> 1,2,3-Tnchlorobenzene ND 10 0 5 1,2,4-Tnehlorobenzene ND 1 0 0-5 <br />' 1,1,1-Trichloroethane ND 10 E 05 1 1,2-Trichloroethane ND 1 0 05 <br /> Trichloroethene ND 10 05 Trichlorofluoromethane ND 1 0 05 <br /> 1,2,3-Trichloropro ane ND 1 0 0 5 1,1,2-Trichloro-1,2,2-tnfluoroethane ND 1 0 10 <br /> 1,2,4-Trimethylbenzene ND l 0 0 5 1,3,5-Tnmeth (benzene ND 1 0 0 5 <br />' <br /> Vinyl Chloride ND 1 0 0 5 X lens ND 10 05 <br /> Surrogate Recoveries(%) <br /> %SSI 117 %SS2 910 <br /> °/eSS3 81 0 <br />' Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported inµgll-,soil/sludge/solid samples in pg/kg, wipe samples inµglwrpe, <br /> production/non-aqueous liquid samples in mg1L <br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br />' h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—1 vol %sediment,l)sample diluted due to high <br /> organic content <br /> 1i <br /> DHS Certification No 1644 ngela Rydehus,Lab Manager <br />