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110 2nd Avenue South #D7 Pacheco,CA 94553 5560 <br /> McCampbell Analytical Inc Telephone 925-798 1620 Fax 925 798-1622 <br /> ht /lwww rrnca bel]com E-mail main mcca bell e,om I <br /> Advanced GeoEnvironmental, Inc Client Project ID Cherokee Truck Stop Date Sampled 09/25/03 <br /> 837 Shaw Road Date Received 09/26/03 <br /> Client Contact Paul Dotson Date Extracted 09/30/03-10/01/03 <br /> Stockton,CA 95215 <br /> Clie�PO [Date Analyzed 09130103-10101103 <br /> Volatiles Organics+Oxygenates by P&T and GC/MS(Basic Target List)* <br /> Extraction Method, SW5030B Analytical Method SW9260B Work Order 0309482 <br /> Lab ID 0309482-OOI C <br /> Client ID UST2 <br /> Matrix Water <br /> Compound Concentration* DF R`L,mt Compound Concentration DF k�rt>ng <br /> * t.trtltE <br /> Acetone ND 10 50 tert-Am l meth i ether(TAME ND 1 0 0 5 <br /> Benzene ND 10 0 5 Bromobenzene ND l 0 0 5 <br /> Bromochloromethane ND 10 0 5 1 Bromodichloromethane ND 1 0 0 5 <br /> Bromoform ND 10 0 5 Bromomethane ND 1 0 0 5 <br /> 2-Butanone(MEK) ND l 0 1 0 t-But I alcohol A) ND 1 0 5 0 <br /> n-But 1 benzene ND l 0 0 5 sec-Butyl benzene ND 1 0 0 5 <br /> tert-Bu l benzene i ND 1 0 0 5 Carbon Disuiftde ND I D 0 5 <br /> Carbon Tetrachloride ND l 0 0 5 Chlorobenzene ND 1 0 0 5 <br /> Chloroethane ND l 0 0 5 2-Chloroeth 1 Vinyl Ether ND 1 0 0 5 <br /> Chloroform ND l 0 0 5 Chloromethane ND 1 0 0 5 <br /> 2-Chlorotoluene ND to 0 5 4-Chlorotoluene ND 1 0 0 5 <br /> Dibromochioromethane ND 10 0 5 1,2-Dibromo-3-chloropro ane ND 1 0 0 5 <br /> 1,2-Dibromoethane EDB) ND 10 0 5 Dibromomethane ND 1 0 0 5 <br /> 1,2-Dichlorobenzene ND 10 0 5 1 3-Dichlorobenzene ND 1 0 0 5 <br /> 1,4-Dichlorobenzene ND 10 0 5 Dichlorodifluoromethane ND 10 0 5 <br /> 1,1-Dichloroethane ND 10 0 5 1,2-Dichloroethane(1,2-DCA) ND 1 0 0 5 <br /> 1,1-Dichloroethene ND 10 0 5 cis-1,2-Dichloroethene ND 1 0 0 5 <br /> trans-1 2-Dichloroethene ND 10 0 5 1,2-Dichloro ro ane ND 1 0 0 5 <br /> 1,3-Dichloropro ane ND 10 0 5 2,2-Dichloro ro ane ND l 0 0 5 <br /> 1,1-Dichlorora ene ND 10 0 5 cis-1,3-Dichloro ro ene ND 10 0 5 <br /> trans-l,3-Dichloro ro ene ND 1 0 0 5 Dusopro l ether(DIPS) ND l 0 0 5 <br /> Ethylbenzene ND 1 0 0 5 Ethyl Cert-butyl ether(ETBE) ND 1 0 0 5 <br /> Hexachlorobutadiene ND 10 0 5 2-Hexanone ND 1 0 0 5 <br /> l4- <br /> domethane Meth 1 iodide ND 1 0 5 0 Isoprop lbenzene ND 1 0 0 5 <br /> Iso rot toluene ND 1 0 0 5 Meth 1-t-butyl ether MTBE ND 10 0 5 <br /> ethylene chloride ND 10 0-5 4-Meth 1-2- entanone(MIRK) ND 10 0 5 <br /> Naphthalene ND 1 0 0 5 _a:Erupyl.benzene ND 1 0 0 5 <br /> Styrene ND 1 0 0 5 1 1,1,1 2-Tetrai,hioroethane ND 1 0 0 5 <br /> 1,1,2 2-Tetrachloroethane ND l 0 0 5 1 Tetrachloroethene ND 1 0 0 5 <br /> Toluene ND 1 0 0 5 1,2,3-Tnehlorobenzene ND 1 0 0 5 <br /> 1,2,4-Trichlorobenzene ND 1 0 0 5 1 1,1-Trichloroethane ND 1 0 0 5 <br /> I 1,1,2-Trichloroethane ND 1 0 0 5 Trichloroethene ND 1 0 0 5 <br /> Tnchlorofluoromethane ND 10 0 5 1,2 3-Tnehloro ro ane ND 1 0 0 5 <br /> 1,2,4-Trimeth lbenzene ND 10 0 5 1,3,5-Tnmeth lbenzene ND 1 0 0 5 <br /> Vinyl Acetate ND 10 50 Vinyl Chloride ND 1 0 0 5 <br /> X lenes ND 1 0 0 5 <br /> Surrogate Recoveries(%) <br /> %SSI 114 %SS2 101 <br /> %SS3 941 <br /> Comments <br /> "water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soiVsludge/solid samples inµglkg, wipe samples inµg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate ooelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Angela Rydelius,Lab Manager <br />