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' 110 2nd Avenue South #D7 Pacheco CA 94553-SSGD z <br /> McCalmpbell Analytical Inc Telephone 925-798-1620 Fax 925 798-1622 <br /> htq�/lwww mcc bell com E rriail roam maccampbell com <br />' Advanced GeoEnvixonmental, Inc Client Project ID Cherokee Truck Stop Date Sampled 09/25/03 <br /> . 837 Shaw Road Date Received 09/26/03 <br />' Client Contact Paul Dotson Date Extracted 09/30/03-10/01/03 <br /> Stockton, CA 95215 <br /> Client P O Date Analyzed 09/30/03-10/01/03 <br />' Volatiles Organics+Oxygenates by P&T and GUMS(Basic Target List)* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0309482 <br /> Lab 1D 0309482-003C <br />' Client M UST4 <br /> Matrix Water <br /> Compound Concentration* DF Re',—.0t g Compound Concentration* DF P wUm"mg <br />' Acetone ND 1 0 1 50 tert-Am 1 methyl ether TAME ND 10 05 <br /> Benzene ND 1 0 05 Bromobenzene ND l 0 05 <br /> Bromochloromethane ND 1 0 05 Brumodichloromethane ND 1 0 05 <br /> Bromoform ND 1 0 0 5 Bromomethane ND 1 0 05 <br />' 2-Butanone(MEK) ND 1 0 1 0 t-Butyl alcohol(TBA ND 1 0 50 <br /> n-Butyl benzene ND 1 0 0 5 sec-Butyl benzene ND 1 0 05 <br /> tert-But 1 benzene ND 10 0 5 Carbon Disulfide ND it0 0 5 <br /> Carbon Tetrachloride ND 1 0 05 Chlorobenzene ND ] 0 0 5 <br />' Chloroethane ND to 0 5 2 Chloroethyl Vinyl Ether ND ] 0 0 5 <br /> Chloroform ND to 05 Chloromethane ND 1 0 T70 5 <br /> 2-Chlorotoluene ND 10 0 5 14 Chlorotoluene ND 1 0 0 5 <br /> Dibromochloromethane ND 10 0 5 1 2-Dibromo-3-chloro ra ane ND 10 o5 <br />' 1,2-Dibromoethane EDB ND 1 0 0 5 Dibromomethane ND 1 0 05 <br /> 1 2-Dichlorobenzene ND 1 0 0 5 1,3-Dichlorobenzene ND 1 0 05 <br /> 1,4-Dichlorobenzene ND 1 0 05 Dichlorodifluoromethane ND 1 0 05 <br />' . 1 1-1)ichlowethane ND l 0 0 5 1,2-Dlchloroethane(1,2-DCA ND 1 0 ')5 <br /> 1,1-Dichloroethene ND l0 05 cis-1,2-Dtehloroelhene ND 10 05 <br /> trans-l,2-Dichloroethene ND 1 0 0 5 1,2-DiLhloro roane ND 1 0 0 5 <br /> 1,3-Dichloro ropane ND 10 0 5 2,2-Dichloropro ane ND 1 0 0 5 <br />' 1,1-Dichloro ro ene ND l 0 0 5 cis-1,3-Dichloro ropene ND 1 0 0 5 <br /> trans-l,3-Dichloro ro ent, ND 1 0 0 5 Dnso ro 1 ether(DIPS) ND 1 0 0 5 <br /> Eth Ibenzene ND to 0 5 Eth i tert-butyl ether ETRE ND 10 0 5 <br /> 1-Iexachlorabutadiene ND 10 0 5 2-Hexanone ND 10 05 <br /> t Iodomethane Methyl iodide ND l 0 5 0 Isopropylbenzene ND 1 0 05 <br /> 4-Isopropyl toluene ND 10 0 5 Methyl-t-but l ether MTBE ND 1 0 0 5 <br /> Meth leve chlonde ND 10 0 5 4-Meth 1-2- entanone(MIRK) ND 1 0 05 <br /> Naphthalene ND 10 0 5 n-Propyl benzene ND to 0 5 <br />' S ene ND 1 0 0 5 1,1,1,2-Tetrachloroethane ND 1 0 0 5 <br /> 1,1,2,2-Tetrachloroethane ND 10 05 Tetrachloroethene ND 10 05 <br /> Toluene ND 1 0 0 5 1,2 3-Trichlorobenzene ND 1 0 0 5 <br /> 1,2,4-Tnehlorobenzene ND 1 0 0 5 1 1,1-Trichloroethane ND 1 0 0 D <br />' 1,1,2-Trichloroethane ND 1 0 0 5 Trichloroethene ND 1 0 0 5 <br /> Tnehlorofluoromethane ND 1 0 0 5 1,2,3-Trichloro ro ane ND 1 0 0 5 <br /> 1,2,4-Tnmeth lbenzene ND 1 0 0 5 1,3,5-Tnmeth Ibenzene ND 1 0 0 <br /> Vinyl Acetate ND 1 0 5 0 Vinyl Chloride ' ND 1 0 05 <br />' Xvlenes I ND l 0 0 5 <br /> Surrogate Recoveries(%) <br /> %SSI III %SS2 95 3 <br />' %SS3 984 <br /> Comments <br /> •water and vapor samples and all TCLP&SPLP extracts are reported in pg/L,soil/sludge/solid samples in gglkg, wipe samples inµg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br />' ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> .#surrogate diluted out of range or surrogate coelutes with another peak <br />' h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content <br />' DHS Certification No 1644 Angela Rydehus, Lab Manager <br />