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13 February 1997 <br /> AGE-NC Project No. 97-0298 <br /> Page 4 of 5 <br /> data. <br /> 4. Decontaminate sampling equipment in an Alconox solution and rinse with water prior to <br /> each sampling run. <br /> 5. Obtain soil gas samples at depths of 10 and selectively at 20 feet bsg. Samples will be <br /> collected using a Geoprobe soil vapor assembly. <br /> 6. An expendable vapor point will be placed into a point holder at the bottom of a string of 1- <br /> inch diameter hollow drive rods. The assembly NN•ill then be advanced to the specified depth <br /> and retracted between six inches in order to engage the expendable point and expose a <br /> column of strata from which soil gas can be extracted. <br /> 7. A post run tubing adapter equipped .with an O-ring to ensure a vacuum-tight seal is then <br /> attached to a'/4-inch diameter,single use,disposable polyethylene tubing. The sampling tube <br /> is then lowered through the center of the hollow drive rods and secured by threading into tine <br /> expendable point holder. <br /> 8. Above ground, the polyethylene tubing is attached to a stainless steel T-valve. This T-valve <br /> is then connected to Vacuum pump contained within the GeoProbe 5400 soil sampling <br /> machine. <br /> 9. The vacuum pump will then be used to apply a negative pressure to the exposed soil column <br /> until approximately three volunes of soil vapor or ambient air is evacuated through the <br /> sampling system. <br /> 10. At the sampling point, a Tedlar bag will placed into a vacuum chan;ber. The sampling tube <br /> will be attached directly to the Tedlar sampling bag,through a collapsible, air tight port. The <br /> vacuum chamber is then sealed, a negative pressure is applied to the chamber by the vacuum <br /> pump. The Tedlar bag will be filled, allowing the sample to enter directly into the Tedlar <br /> bag. On complete collection of the gas sample, the negative pressure in the chamber is <br /> reduced, the sampling bag sealed. <br /> 11. Upon collection, label each sample, log on chain-of-custody and place into a dry cooler. <br /> 12. Soil gas from the polyethylene tubing is then monitored for the presence of volatile organics <br /> using a photo-ionization detector (PID) pre-calibrated to isobutylene. <br /> 13. Deliver samples to an on-site chemist for direct injection into a State-certified mobile <br /> laboratory for analysis by EPA methods 8010 and 8020, which includes all target <br /> compounds. <br /> 14. Backfill each probe boring on the site to surface grade using Portland Cement. <br />