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Ain an Environtneti..ta [Network <br /> WORK ORDER: 9711230 QUALITY CONTROL REPORT PAGE QR-2 <br /> ANALYSIS:. Gasoline Oxygenates <br /> MATRIX: Water <br /> METHOD BLANK SAMPLES <br /> .................. ..... .-- --- ---- --... ----- --- ---------------------- <br /> SAMPLE TYPE: Blank-Method/Media.blank LAB ID: BLNK_1124 INSTR RUN: GCMS13\971124200000/1/ <br /> INSTRUMENT: HP mass spec for Volatiles PREPARED: BATCH ID: MS13W112597 <br /> UNITS: ug/L ANALYZED: 11/24/97 DILUTION: 1.00 <br /> METHOD: <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1,2-DCE-d4 (surr) 94.8 100 100 94.8 70 130 <br /> Toluene-d8 (surr) 98.2 100 100 98.2 70 130 <br /> Bromofluorobenzene (surr) 93.5 100 100 93.5 70 130 <br /> Methy•t-butyl ether (MTBE) ND 5 <br /> Ethyl-t-butyl ether (ETBE) ND 5 <br /> t-Amylmethyl ether (TAME) ND 5 <br /> t-Butanol (TBA) ND 100 <br /> Di-isopropyl ether (DIPE) NO 5 <br /> LABORATORY CONTROL SAMPLES <br /> ----------------------------------------------------------------------------------------------------------------------•••-- <br /> SAMPLE TYPE: Laboratory Control Spike LAB ID: LCS 1125 INSTR RUN: GCMS13\971124200000/4/1 <br /> INSTRUMENT: HP mass spec for Volatiles PREPARED: — BATCH ID: MS13W112597 <br /> UNITS: <br /> ug/L ANALYZED: 11/25/97 DILUTION: 1.00 <br /> METHOREF REPORTING . SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1,2-DCE-d4 (surr) 94.1 94.8 100 100 94.1 70 130 <br /> Toluene-d8 (surr) 104 98.2 100 100 104 70 130 <br /> Bromofluorobenzene (surr) 81.9 93.5 100 100 81.9 70 130 <br /> Methy-t-butyl ether (MTBE) 97.7 ND 5 100 97.7 32 158 <br /> Ethyl-t•butyl ether (ETRE) 111 ND 5 100 111 32 158 <br /> t-Amylmethyl ether (TAME) 100 ND 5 100 100 32 158 <br /> .................... -----.....------------... <br /> SAMPLE SURROGATES <br /> ...... ..... ..................... --- --- ........... <br /> SAMPLE-TYPE:-Sample-Client LAB ID: 9711230.04A INSTR RUN: GCMS13\971124200000/17/ <br /> INSTRUMENT: HP mass spec for Volatiles PREPARED: BATCH ID: MS13W112597 <br /> UNITS: ug/L ANALYZED: 11/28/97 DILUTION: 1.00 <br /> METHOD: <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1,2-DCE-d4 (surr) 92.5 100 100 92..5 70 130 <br /> Toluene-d8 (surr) 103 100 100 103 70 130 <br /> Bromofluorobenzene (surr) 84.4 100 100 84.4 70 130 <br /> ----...-----••----------------------------•---.....----......----------- -----•---------•--------------••------- ............ <br /> SAMPLE TYPE: Sample-Client LAB ID: 9711230-08D INSTR RUN: GCMS13\971124200000/15/ <br /> r INSTRUMENT: HP mass spec for Volatiles PREPARED: BATCH ID: MS13W112597 <br /> L UNITS: ug/L ANALYZED: 11/26/97 DILUTION: 5.00 <br /> METHOD: <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1.2•DCE-d4 (surr) 91.4 500 100 91.4 70 130 <br /> Toluene-d8 (surr) 103 500 100 103 70 130 <br /> Bromofluorobenzene (surr) 91.2 500 100 91.2 70 130 <br /> r -----------------------•----------...--•---....................-----------••-------------•-----..........----......---..---•- <br /> 4� <br />