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I 10 2nd Avenue South, #D7,Pacheco,CA 94553-5560 <br /> McCAWBELL ANALYTICAL INC Tviephone 925-798-1620 Fax 925-798-1622 <br /> htto//www mccam bell cora E-mail main@a mccampbell corn <br /> Advanced GeoEnvironmental Client Project ID West Clay Date Sampled 02/27/2002 <br /> 837 Shaw Road Date Received 02/28/2002 <br /> rStockton, CA 95215 Chent Contact Paul Dotson [Date Extracted 02/28/2002 <br /> Client P O Date Analyzed_ 02/28/2002 <br /> Seven) Oxygenated Volatile Organics By GC/MS <br /> �;k method 3260 modified <br /> Lab 1D 0202184- 0202184 0202184 0202184 <br /> 001 002 003 004 <br /> MWl/ ,vfw2,/ MW3/ MW4/ Reporting Limit <br /> tID 022702 022702 022702 022702 <br /> Ma= W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Dr-isopropyl Ethe-(DIPE) ND ND ND ND 5 0 10 <br /> Ethyl tett-Butyl Ether(ETBF) ND ND ND NO 50 10 <br /> Methyl tern-Bury)Ether(MTBE) ND ND ND ND 50 10 <br /> test-Amyl Methyl Ether(TAME) ND ND ND ND 50 to I <br /> tert-Butanol ND ND ND ND 25 50 <br /> r <br /> Methanol ND ND ND ND 2500 a00 <br /> I <br /> Ethanol ND ND ND ND 250 50 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 101 106 101 106 <br /> Comments <br /> "water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting hrrut,NIA means surrogate not appiicable to this analysis <br /> (h)lighter than water immiscible sneen is present,(i)liquid sample that contains greater than--5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />