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110 2nd Avenue South,#D7,Pacheco, CA 94553-5560 <br /> McCATNOBELL ANALYTICAL INC Telenhone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell cazii E-mail main@mccampbell corn <br />' Advanced GeoEnvironmental Client Project ID West Clay Date Sampled 02/27/2002 <br /> 837 Shaw Road Date Received. 02/28/2002 <br />' Stockton, CA 95215 CIient Contact Paul Dotson Date Extracted 02/28/2002 <br /> Client P O Date Analyzed 02/28/2002 <br /> Seven Oxygenates/ Volatile Organics By GC/MS i <br /> EPA method 8260 madtfied <br /> Lab M 0202I84- 0202184 0202184- 0202184- <br /> 013 <br /> 202184013 014 015 016 <br /> MW I l A/ MW 11B/ MW 12A/ MW 128/ Reportnig L mit <br /> Client ID 022702 022702 022702 022702 <br /> Matrix W W W W S W <br /> Compound Concentration' ug/kg 1glL <br /> Dt-,sapropyl Ether(DIPa) ND � ND ND ND 50 1 0 <br /> Ethyl tern-Butyl Ether(ETRE) ND ND i ND ND 50 1 0 <br /> Methyl tent-Butyl Ether(MTBE) ND 17 ND 19 { 50 1 0 <br /> i � <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 50 10 <br /> itert-Butanol ND ND � ND ivlD 25 50 <br /> i Methanol ND ND ND ND 2500 500 <br /> i <br /> Ethanol ND ND ND ND 250 50 <br /> i <br /> Surrogate Recoveries(%) <br /> iDthromotluortsmethane 108 105 105 105 <br /> iComments <br /> i *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/vipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysts <br /> (h)lighter than water inin sc.ble sheen is present,(i)liquid sample that contains greater than--5 vol %sediment,0)sample diluted due to <br /> high organic conte-tt <br /> DHS Certification No 1644Edward Hamilton,Lab Director <br />