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110 2nd Avenue South,#D7,Pacheco, CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampizgll co m E-mail main@mccampbell com <br /> I <br /> Advanced GeoEnvironmental Client Project ID West Clay Prop Date Sampled 11/28/01 <br />' 837 Shaw Road Date Received 11/28/01 <br /> Stockton, CA 95215 Client Contact Paul Dotson Date Extracted 11/30-12/03/01 <br /> Client P O Date Analyzed 11/30-12/03/01 <br /> i <br /> Seven Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 84436 84437 84438 84439 <br /> MW13A/11- MW13B/11- EW-1/11- EW-2/11- Reporting Limit <br /> Client ID 28-01 28-01 28-01 28-01 <br /> Matrix W W W W 5 W <br /> Compound Concentration* ug/kg I ag/L <br /> Dt-isopropyl Ether(D1PE) ND ND ND<5 0 ND so 1 0 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND ND<5 0 ND 50 1 0 <br />�. Methyl Cert-Butyl Ether(MTBE) 22 37 340 ND 50 1 0 <br /> ftent-Amyl Methyl.Ether(TAME) ND ND ND<5 0 ND 50 1 0 <br /> tert-Butanol ND ND ND<25 ND 25 5 0 <br /> Methanol ND ND 2500 500 <br /> IEthanol ND ND ND<250 ND 250 50 <br /> ESurrogate Recoveries(°/,P) <br /> Dibromotluoiomethane 102 102 94 103 <br /> Comments <br /> *water samples are reported in ug/t.,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present (i)liquid sample that contains greatei than —5 voi %sediment 0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />