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1 <br /> 1102nd Avenue South,#D7,Pacheco,CA 94553-5560 <br />' McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http_//www mccampbell corn E-mail main@mccampbell com <br /> • <br />' Advanced GeoEnvironmental Client Project ID West Clay Properties Date Sampled 12/18/00 <br /> 4005 North Wilson Way Date Received 12/18/00 <br />' Stockton, CA 95205 Client Contact Paul Dotson Date Extracted 12119-12/22/00 <br />' Client P O Date Analyzed 12/19-12/22/00 <br /> 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br />' Lab ID 56299 56300 56301 56302 <br /> MW11A/ MW11B/ MW12A/ MW12B/ Reporting Limit <br /> Client ID 12-18-00 12-18-00 12-18-00 12-18-00 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPE) ND ND ND ND 50 1 0 <br />' Ethyl tert-Butyl Ether(ETBE) ND ND ND ND 50 10 <br />' Methyl-tent Butyl Ether(MTBE) ND 30 ND 55 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 50 to <br /> ftert-Butanol ND 68 ND ND 25 so <br /> Methanol ND ND ND ND 1000 200 <br /> Ethanol ND ND ND 170 250 50 <br /> Surrogate Recoveries <br />' Dtbromofluoromethane 107 106 106 107 <br /> IComments <br /> *water samples are reported to uglL,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 *Edward Hamilton,Lab Director <br />