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110 2nd Avenue South #137 Pacheco CA 94553-5560 <br /> Mir ° McCampbell Analytical, Inc. Telephone 925-798-1620 Fax 925 798 1622 <br /> Website www mccarripbell com E mail mamQmccampbell corn <br /> i� <br /> Advanced GeoEnvironmental,Inc Client Project ID West Clay-Ozone Date Sampled 04/01/05 <br /> BST Date Received 04/05/05 <br /> 837 Shaw Road <br /> Client Contact Bill Little Date Extracted 04/05/05 <br /> Stockton, CA 95215 Client P O Date Analyzed 04/07/05 <br /> Volatile Organics by P&T and GUMS(Basic Target List)'* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0504049 <br /> Lab ID 0504049-001 A <br /> Client ID Soil Initial <br /> Matrix Reporting Soil <br /> Am <br /> s <br /> Compound Concentration DF Compound Concentration* DF T-Inut i <br /> Acetone ND<10 200 005 Acrolem(Propenal) ND<10 200 005 <br /> Acrylonitnle ND<4 0 200 002 tert-Am 1 methyl ether(TAME) ND<1 0 200 0 005 <br /> Benzene ND<1 0 200 0 005 Bromobenzene ND<1 0 200 0 005 <br /> Bromochloromethane ND<1 0 200 0 005 Bromodichloromethane ND<1 0 200 0 005 <br /> Bromoform ND<1 0 200 0 005 Bromomethane ND<1 0 200 0 005 <br /> 2-Butanone MEK) ND<4 0 200 002 t-But l alcohol(TBA) ND<5 0 200 0 025 <br /> n-But 1 benzene 6 8 200 1 0 005 sec-Butyl benzene 1 8 200 0 005 <br /> tert-But l benzene ND<1 0 200 0 005 Carbon Disulfide ND<l 0 200 0 005 <br /> Carbon Tetrachloride ND<l 0 200 0 005 Chlorobenzene ND<1 0 200 0 005 <br /> Chloroethane ND<l 0 200 0 005 2-Chloroeth 1 Vinyl Ether ND<2 0 200 0 01 <br /> Chloroform ND<1 0 200 0 005 Chloromethane ND<1 0 200 0 005 <br /> 2-Chlorotoluene ND<1 0 200 0 005 4-Chlorotoluene ND<1 0 200 0 005 <br /> Dibromochloromethane ND<1 0 200 0 005 1,2-Dibromo-3-chloro ro ane ND<1 0 200 0 005 <br /> 1,2-Dibromoethane(EDB) ND<l 0 200 0 005 Dibromomethane ND<1 0 200 0 005 <br /> 1,2-Dichlorobenzene ND<1 0 200 0 005 1,3-Dichlorobenzene ND<1 0 200 0 005 <br /> 1,4-Dichlorobenzene ND<1 0 200 0 005 Dichlorodifluoromethane ND<l 0 200 0 005 <br /> 1,1-Dichloroethane ND<1 0 200 0 005 1,2-Dtchloroethane 1,2-DCA ND<1 0 200 0 005 <br /> I,1-Dichloroethene ND<1 0 200 0 005 cis-1,2-Dichloroethene ND<1 0 200 0 005 <br /> trans-l,2-Dn,hloroethene ND<l 0 200 0 005 1,2-Dichloro ro ane ND<1 0 200 0 005 <br /> 1,3-Dichloro ro ane ND<l 0 200 0 005 2,2-Dichloro ro ane ND<1 0 200 0 005 <br /> 1,1-Dichloro ro ene ND<10 200 0005 cis-1,3-Dlchloro ro ene ND<10 200 0005 <br /> trans-1,3 Dichloro ro ene ND<1 0 200 0 005 Diiso ro 1 ether(DIPE) ND<1 0 200 0 005 <br /> Eth lbenzene 16 200 0 005 Ethyl ten-butyl ether(ETBE) ND<1 0 200 0 005 <br /> Freon 113 ND<20 200 1 0 1 Hexachlorobutadiene ND<1 0 200 0 005 <br /> Hexachlomethane ND<l 0 200 0 005 2-Hexanone ND<1 0 200 0 005 <br /> Iso ro ylbenzene 2 2 200 0 005 4-11sopropyl.toluene ND<1 0 200 0 005 <br /> Meth 1-t-butyl ether MTBE ND<1 0 200 0 005 Methylene chloride ND<l 0 200 0 005 <br /> 4-Meth 1-2- entanone(MIRK) ND<1 0 200 0 005 Naphthalene 9 4 200 0 005 <br /> Nitrobenzene ND<20 200 0 1 n-Propyl benzene 9 6 200 0 005 <br /> Styrene ND<1 0 200 0 005 1,1,1,2-Tetrachloroethane ND<1 0 200 0 005 <br /> 1,1,2,2-Tetrachloroethane ND<1 0 200 0 005 Tetrachloroethene ND<1 0 200 0 005 <br /> Toluene ND<l 0 200 0 005 1,2,3-Tnchlorobenzene ND<1 0 200 0 005 <br /> 1,2,4-Trichlorobenzene ND<10 200 0005 1,1,1-Tnchloroethane ND<10 200 0005 <br /> 1,1,2-Trichloroethane ND<1 0 200 0 005 Trichloroethene ND<1 0 200 0 005 <br /> Trichlorofluoromethane ND<1 0 200 0 005 1,2,3-Tnchloro ro ane ND<1 0 200 0 005 <br /> 1,2 4-Tnmeth ]benzene 43 200 0 005 1,3,5-Trimeth lbenzene 2 l 200 0 005 <br /> Vinyl Chloride ND<1 0 200 0 005 Xylenes 59 200 0 005 <br /> Surrogate Recoveries(%) <br /> %SSI 88 %SS2 85 <br /> %SS3 100 <br /> Comments <br /> *water and vapor samples are reported in pglL,soil/sludge/solid samples in mg/kg,product/oillnon-aqueous liquid samples and all TCLP&SPLP <br /> extracts are reported in mg/L,wipe samples in pg/wipe <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--1 vol %sediment,))sample diluted due to high <br /> organic contentlmatnx interference,k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight,m) <br /> reporting limit raised due to insufficient sample amount,n results are re orted on a dry weight basis, see attached narrative <br /> DHS Certification No 16440 0 Angela Rydebus, Lab Manager <br />