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110 2nd Avenue South #D7 Pacheco CA 94553 5560 McCampbell Analytical, Inc. Telephone 925-798-1620 Fax 925 798-1622 Websde www mecampbell com E mail mam®mecampbell com • Advanced GeoEnvtronmental,Inc Client Project ID West Clay-Ozone Date Sampled 04/05/05 BST Date Received 04/05/05 837 Shaw Road Client Contact Bill Little Date Extracted 44/13/05 Stockton,CA 95215 Client P O Date Analyzed 04/13/05 Volatile Organics by P&T and GUMS(Basic Target List)* Extraction Method SW50308 Analytical Method SW826013 Work Order 0504049 Lab ID 0504049-007A Client ID Water Final Matrix Water e run Compound Concentration* DF RUnvt a Compound Concentration * DF i g Acetone 1200 10 50 1 Acrolem(Propenal) ND<50 10 50 Acrylonitrile ND<20 10 20 tert-Am 1 methyl ether(TAME) ND<5 0 10 05 Benzene 2 9 10 0 5 Bromobenzene ND<5 0 10 0 5 Bromochloromethane ND<5 0 10 0 5 BrOmodichloromethane ND<5 0 10 0 5 Bromofonn ND<5 0 10 0 5 Bromomethane ND<5 0 10 0 5 2-Butanone(MEK) 360 10 2 0 t-Butyl alcohol(TBA) ND<50 10 5 0 n-But l benzene 20 1 ]0 0 5 sec-Butyl benzene 5 8 ]0 0 5 tert-But 1 benzene ND<5 0 10 0 5 Carbon Disulfide ND<5 0 10 0 5 Carbon Tetrachloride ND<5 0 10 0 5 Chlorobenzene ND<5 0 10 0 5 Chloroethane ND<5 0 V002-Chloroeth l Vm 1 Ether ND<10 10 1 0 Chloroform ND<5 0 Chloromethane ND<5 0 10 0 5 2-Chlorotoluene ND<5 0 4-Chlorotoluene ND<5 0 ]0 0 5 Dibromochlorumethane ND<5 0 1,2-Dibromo-3-chloro ro ane ND<5 0 10 0 5 1,2-Dibromoethane(EDB ND<5 0 Dibromomethane ND<5 0 10 0 5 1,2-Dichlorobenzene ND<5 0 1,3-Dichlorobenzene ND<5 0 10 0 5 1,4-Dichlorobenzene ND<5 0 Dichlorodifluoromethane ND<5 0 10 0 5 i,l-Dichloroethane ND<5 0 10 0 5 1,2-Dichloroethane(1,2-DCA) ND<5 0 10 0 5 1,1-Dichloroethene ND<5 0 10 0 5 cis-1,2-Dichloroethene ND<5 0 10 0 5 trans-1,2-Dichloroethene ND<5 0 10 0 5 1,2-Dtchloro ro ane ND<5 0 10 0 5 1,3-Dichloro ro ane ND<5 0 1 10 0 5 2,2-Dichlororo ane ND<5 0 10 0 5 1,1-Dtchloro ro ene ND<5 0 10 0 5 cis-1 3-Dichloro ro ene ND<5 0 10 0 5 trans-l,3-Di chloro ro ene ND<5 0 10 0 5 DuSOPTUPY1 ether DIPS ND<5 0 10 0 5 Eth lbenzene 100 t0 0 5 Ethyl tert-but l ether ETRE) ND<5 0 10 0 5 Freon 113 ND<100 10 10 Hexachlorobutadiene ND<5 0 10 0 5 Hexachloroethane ND<5 0 10 0 5 2-Hexanone ND<5 0 10 0 5 Isopropylbenzene 14 10 0 5 4-Iso ro ]toluene ND<5 0 10 0 5 Meth l-t-but l ether(MTBE) ND<5 0 10 0 5 Methylene chloride ND<5 0 10 0 5 4-Meth 1-2- entanone(MIBK) ND<5 0 10 0 5 Naphthalene 90 ]0 0 5 Nitrobenzene ND<100 to 10 n-Propyl benzene 53 10 0 5 S ene ND<5 0 10 0 5 1 1 1,2-Tetrachloroethane ND<5 0 10 0 5 1,1 2,2-Tetrachloroethane N13<5 0 10 0 5 Tetrachloroethene ND<5 0 10 0 5 Toiuene ND<5 0 10 0 5 1,2 3-Trichlorobenzene ND<5 0 le 0 5 1,2,4-Trichlorobenzene ND<5 0 10 0 5 1,1 I-Trichloroethane ND<5 0 10 0 5 1,1,2-Trichloroethane ND<5 0 10 0 5 Trichloroethene ND<5 0 10 0 5 Trichlorofluoromethane ND<5 0 10 0 5 1 2,3-Trichloro ro ane ND<5 0 10 0 5 1,2,4-Trimethylbenzene 280 10 0 5 1,3,5-Trimeth ]benzene 14 10 0 5 Vinyl Chloride ND<5 0 10 0 5 1 Xylenes 300 i0 0 5 Surrogate Recoveries(%) %S S 1 94 %SS2 93 %SS3 104 Comments "water and vapor samples are reported in jig/L,soil/sludge/solid samples to mg/kg,producVoil/non-aqueous liquid samples and all TCLP&SPLP extracts are reported in mg/L,wipe samples in Vg/wipe ND means not detected above the reporting limit NIA means analyte not applicable to this analysts #surrogate di luted out of range or surrogate coelutes with another peak h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—1 vol %sediment,j)sample diluted due to high organic content/matrix interference,k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight,m) reporting limit raised due to insufficient sample amount,n results are reported on a dry weight basis, see attached narrative DHS Certification No 1644 u- Angela Rydelius, Lab Manager