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Date: Alp hWa1y tical Inc. - QC Summary R&rt Wok Order: <br /> ' 29-Jun-01 <br /> Method Blank Type MBLK Test Code:SW8260B Batch ID:MS9S0622A <br /> ' File ID: D:\HPCHEM\MS09\DATA\010622\01062208.D Analysis Date: 06/22/2001 12:44 <br /> Sample ID: MBLK MS9S0622A Units:Ng/Kg Run ID:GC/MSD_9_010622B Prep Date: 06/2212001 <br /> Analyte Result PQL SpkVal SpkRefVal %REG LowLimit HighLimit RPD Ref Val %RPD Qual <br /> ' Chloromethane NO 40 <br /> Vinyl chloride NO 20 <br /> Chloroethane NO 20 <br /> Bromomethane NO 20 <br /> ' Trichloro8uoromethane NO 20 <br /> 1,1-Dichloroethene NO 20 <br /> Dichloromethane ND 40 <br /> trans-1,2-Dichloroethene ND 20 <br /> 1,1-Dichlorcethane NO 20 <br /> ' cis-1,2-Dichloroethene NO 20 <br /> Chloroform NO 20 <br /> 1,2-Dichloroethane NO 20 <br /> 1,1,1-Trichloroethane NO 20 <br /> ' Carbon tetrachloride NO 20 <br /> Benzene NO 5 <br /> 1,2-Dichloropropane NO 20 <br /> Trichloroethene NO 20 <br /> ' Bromodichloromethane NO 20 <br /> cis-1,3-Dichloropropene NO 20 <br /> trans-1,3-Dichloropropene NO 20 <br /> 1,12-Trichloroethane NO 20 <br /> Toluene NO 5 <br /> ' Dibromochloromethane ND 20 <br /> Tetrachloroethene NO 20 <br /> Chlorobenzene NO 20 <br /> Ethylbenzene NO 5 <br /> ' m,p-Xylene NO 5 <br /> Bromoform NO 20 <br /> o-Xylene NO 5 <br /> 1,12,2-Tetrachloroethane NO 20 <br /> ' 1,3-Dichlorobenzene ND 20 <br /> 1,4-Dichlorobenzene NO 20 <br /> 1,2-Dichlorobenzene NO 20 <br /> tLaboratory Control Spike Type LCS Test Code:SW8260B Batch ID:MS9S0622A <br /> File ID:D:\HPCHEM\MS09\DATA\010622\01062230.D Analysis Date: 06/22/2001 20:45 <br /> Sample ID: LCS MS9S0622A Units:pg/Kg Run ID:GC/MSD_9_010622B Prep Date: 06/22/2001 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> 1,1-Dichloroethene 123 20 200 62 0 148 <br /> Benzene 190 5 200 95 32 148 <br /> Trichloroethene 194 20 200 97 17 177 <br /> Toluene 187 5 200 93 39 136 <br /> ' Chlorobenzene 190 20 200 95 27 162 <br /> Ethylbenzene 196 5 200 98 45 152 <br /> m,p-Xylene 387 5 400 97 42 154 <br /> o-Xylene 197 5 200 98 41 154 <br /> ' Sample Matrix Spike Type MS Test Code:SW8260B Batch ID:MS9S0622A <br /> File ID:D:\HPCHEM\MS09\DATA\010622101062232.D Analysis Date: 061221200121:28 <br /> Sample ID: 01062261-03AMS Units:pg/Kg Run ID:GC/MSD_9_010622B Prep Date: 06/22/2001 <br /> ' Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> 1,1-Dichloroethene 336 40 400 0 84 0 148 <br /> Benzene 385 10 400 0 96 32 148 <br /> Trichloroethene 382 40 400 0 95 17 177 <br /> ' Toluene 377 10 400 0 94 39 136 <br /> Chlorobenzene 390 40 400 0 98 27 162 <br /> Ethylbenzene 397 10 400 0 99 45 152 <br /> m,p-Xylene 791 10 800 0 99 42 154 <br /> ' o-Xylene 400 10 400 0 100 41 154 <br />