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Aha Analytical,' 1 cal, Inc. 255 Glendale Ave •Suite 21 •Sparks,Nevada 89431-5778 (775) 355-1044 •(775) 355-0406 FAX• 1-800-283-1183 *Date QC Summary Report warts Order 03042224 I Sample Matrix Spike Type MS Test Code EPA Method SW8260B File ID D 1HPCHEMlMS081DATA1030423103042308 D Batch ID MS8W0423A Analysis Date 04/23/2003 13 31 ' Sample ID 03042224-09AMS Units pg/L Run ID GCIMSD_8_030423A Prep Date 04/2312003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref V2I %RPD Qual 1 1-Dichloroethene 176 2 5 50 0 35 80 120 S Benzene 21 7 1 3 50 0 43 83 119 S ' Trichloroethene 216 2 5 50 0 43 76 127 $ Toluene 199 1 3 50 0 40 80 120 S Chlorobenzene 208 2 5 50 0 42 76 124 S Ethylbenzene 205 1 3 50 0 41 80 120 S ' m p-Xylene 383 1 3 100 0 38 77 124 S o-Xylene 215 13 50 0 43 77 125 S Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8260B ' File ID D1HPCHEMIMS081DATA1030423103042309 D Batch ID—MS8W0423A Analysts Date 04123/2003 13 54 Sample ID 03042224-09AMSD Units pglL Run ID GC/MSD $ 030423A Prep Date 04123/2003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual 11-Dichloroethene 33 2 5 50 0 66 80 120 176 608 S Benzene 375 13 50 0 75 83 119 2168 535 S Trichloroethene 36 2 5 50 0 72 76 127 21 61 499 S Toluene 334 1 3 50 0 67 80 120 199 505 S Chlorobenzene 345 25 50 0 69 76 124 208 494 S ' Ethylbenzene 349 1 3 50 0 70 80 120 2045 522 S m p-Xylene 653 1 3 100 0 65 77 124 3826 522 S o-Xylene 363 1 3 50 0 73 77 125 21 45 51 5 S mments ND-Not Detected at the Reporting Limit D-If the spiked value is<25%of the reference value,recovery should not be calculated S-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matrix B-Analyte detected in the associated Method Blank 1