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Alpha Analytical, Inc. <br /> 255 Glendale Ave •Suite 21 •Sparks,Nevada 89431-5778 <br /> (775)355-1044 •(775)355-0406 FAX • 1-800-283-1183 <br /> ate' 2.)-Apr-03mWork Order-4pr-03 OC Summary Report 03041746 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW8260B <br /> File ID D IHPCHEMIMS091DATA1030421k03042117 D Batch ID MS9S0421A Analysis Date 04/21/2003 15 19 <br /> ' Sample ID 03041746-02AMS Units pg/Kg Run ID GCIMSD_9_030421A Prep Date 091812003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit Highl-imit RPD Ref Val %RPD Qual <br /> 1,1-Dichloroethene 129 20 200 0 65 0 148 <br /> ' Benzene 151 5 200 0 75 32 148 <br /> Tnchloroethene 159 20 200 0 79 17 177 <br /> Toluene 164 5 200 0 82 39 136 <br /> Chlorobenzene 159 20 200 0 80 27 162 <br /> Ethylbenzene 173 5 200 0 86 45 152 <br /> ' m p-Xylene 327 5 400 0 82 42 154 <br /> o-Xylene 160 5 200 0 80 41 154 <br /> Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8260B <br /> ' File ID D kHPCHEMIMS09kDATA1030421103042118 D Batch ID—MS9S0421A Analysis Date 04/2112003 15 42 <br /> Sample ID 03041746-02AMSD Units pg/Kg Run ID GC/MSD 9 030421A Prep Date 04/18/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit Highl-imit RPD Ref Val %RPD Qual <br /> 1 1-Dtchloroethene 113 20 200 0 57 0 148 1293 134 <br /> Benzene 144 5 200 0 72 32 148 1508 4 9 <br /> Trichloroethene 151 20 200 0 75 17 177 158 9 512 <br /> Toluene 155 5 200 0 77 39 136 1635 5 6 <br /> Chlorobenzene 153 20 200 0 77 27 162 1594 393 <br /> Ethylbenzene 165 5 200 0 62 45 152 1729 475 <br /> m p-Xylene 315 5 400 0 79 42 154 3273 376 <br /> o-Xylene 154 5 200 0 77 41 154 1601 375 <br /> Wments ND Not Detected at the Reporting Limit D-If the spiked value is<25%of the reference value,recovery should not be calculated <br /> S-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matnx <br /> B-Analyte detected in the associated Method Blank <br /> t <br />