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I Alpha Analytical, Inc. 255 Glendale Ave •Suite 21 •Sparks,Nevada 8943 1-5 778 (775)355-1044 - (775)355-0406 FAX • 1-800-283-1183 W ate' QC Summary Report Fork Order 25-Apr-03 0304I746 Sample Matrix Spike Type MS Test Code EPA Method SW82608 File ID D IHPCHEMIMS091DATA1030418103041807 D Batch ID MS9W0418A Analysis Date 04118/2003 10 47 ' Sample ID 03041746-10AMS Units yg1L Run ID GCIMSD_9_030418A Prep Date 04/18/2003 Analyte Result PQL SpkVal SpkRefVal %REC LowLlmlt HighLlmlt RPD Ref Val %RPD Qual 1 1-Dlchloroethene 483 25 50 ❑ 97 80 120 Benzene 441 13 50 0 88 80 120 ' Trichloroethene 466 25 50 0 93 62 137 Toluene 457 1 3 50 0 91 80 120 Chlorobenzene 443 2 5 50 0 89 80 121 Ethylbenzene 478 1 3 50 0 96 80 120 ' m p-Xylene 872 1 3 100 0 87 73 129 o-Xylene 435 1 3 50 0 87 73 127 Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8260B ' File ID D IHPCHEM%MS091DATA1030418103041808 D Batch IDMS9W0416A Analysis Date 04/18/2003 11 10 Sample ID 03041746-10AMSD Units pg1L Run ID GC/MSD-9-030418A Prep Date 04/18/2003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imlt HighLimlt RPD Ref Val %RPD Qual ' 1 1-Dlc1loroe1hene 458 25 50 0 92 80 120 4831 542 Benzene 423 1 3 50 0 85 80 120 441 419 Trichloroethene 439 2 5 50 0 88 62 137 4656 584 Toluene 44 1 3 50 0 88 80 120 45 67 3 75 Chlorobenzene 428 2 5 50 0 86 80 121 4427 349 tEthylbenzene 461 1 3 50 0 92 80 120 4776 3 62 m p-Xylene 836 1 3 100 0 84 73 129 872 426 o Xylene 423 1 3 50 0 85 73 127 4349 2 75 10 minents ND-Not Detected at the Reporting Limit D If the spiked value is<25%of the reterence value,recovery should not be calculated 5-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matrix B-Analyte detected to the associated Method Blank 1 1 ^ I 1 1