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®� STL Submission#:2003-09-0088 <br /> • Semi-volatile analysis by GC/MS - EPA8270C <br /> Blaine Tech Services, Inc. <br /> Attn.: Leon Gearhart <br /> 1680 Rogers Avenue <br /> San Jose, CA 95112-1105 <br /> Phone: (408)573-0555 Fax: (408)573-7771 <br /> Project: 030903-JB 1 Received: 09/03/2003 17:55 <br /> 97093419 <br /> Site: 1267 Country Club Blvd., Stockton <br /> •y.( s a s[ '}cs„-},� : <br /> 3p, kF - 54` F42� A�'3 . - "Y'R�"YF f yk h'� <br /> LC$17 2. .... J08-01::1`1 0 . FFF tf e�°as1381 0 3 AnaiSrzecl .. S.r�7 <br /> Compound Conc. ug/L Exp.Conc. Recovery% RPD Ctrl.Limits% Flags <br /> LCS LCSD LCS LCSD % Rec. RPD LCS LCSD <br /> . Phenol 17.2 18.2 60.0 28.7 30.3 5.4 12-89 35 <br /> 2-Chlorophenol 42.9 44.3 60.0 71.5 73.8 3.2 23-134 25 <br /> 1,4-Dichlorobenzene 16.7 17.3 30.0 55.7 57.7 3.5 36-97 30 <br /> N-Nitroso-di-n-propylamine 21.5 23.9 30.0 71.7 79.7 10.6 10-130 34 <br /> 1,2,4-Trichlorobenzene 18.6 19.3 30.0 62.0 64.3 3.6 44-142 35 <br /> 4-Chloro-3-methylphenol 49.6 49.9 60.0 82.7 83.2 0.6 22-147 31 <br /> Acenaphthene 21.0 23.3 30.0 70.0 77.7 10.4 56-118 30 <br /> 4-Nitrophenol 21.2 18.6 60.0 35.3 31.0 13.0 1-132 35 <br /> 2,4-Dinitrotoluene 25.4 26.4 30.0 84.7 88.0 3.8 39-139 35 <br /> Pentachlorophenol 41.2 38.0 60.0 68.7 63.3 8.2 45-125 35 <br /> Pyrene 24.3 25.2 30.0 81.0 84.0 3.6 52-115 35 <br /> Surrogafes(s) <br /> Nitrobenzene-d5 16.8 18.0 25 67.2 72.0 35114 <br /> 2-Fluorobiphenyl 16.9 18.0 25 67.6 72.0 43-116 <br /> p-Terphenyl-d14 20.7 21.7 25 82.8 86.8 33-141 <br /> 2-Fluorophenol 21.0 21.8 50 42.0 43.6 25-100 <br /> Phenol-d6 15.9 16.3 50 31.8 32.6 10-110 <br /> 2,4,6-Tribromophenol 37.6 137.4 150 75.2 174.8 1 10-123 <br /> I 1125!2003 08:35 <br /> Sevem Trent Laboratories, Inc. <br /> STL San Francisco*1220 Quarry Lane,Pleasanton,CA 94566 Page 4 of 5 <br /> A pm1dSe-Om UW Fac Tel 925 4841919 Fax 925 484 1096`www.stl-inc.com`CA DHS FLAP#2496 <br />