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Report Number: 33211 QC Report : Matrix Spike/ Matrix Spike Duplicate Datel: 5/29/2003 Project Name : 1267 Country Club Project Number: 0305144132 Duplicate Spiked 11 Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample, Relative Percent Percent Spiked Sample Spike Dup. Sample Sample Analysis Date Percent Percent Percent Recov. Diff. Parameter Sample Value Level Level Value. Value Units Method Analyzed Recov. Recov.11 Diff. Limit Limit TPH as Diesel Blank <50 1000 1000 1050 1080 uglL M EPA 8015 5124103 105 108 2.47 70-130 25 Benzene 33219-03 3.3 39.8 39.9 40.1 39.5 ug/L EPA 8260B 5125103 92.3 90.6 1.84 70-130 25 Toluene 33219-03 0.53 39.8 39.9 37.9 37.9 ug/L EPA 8260B 5125103 93.8 93.5 0.291 70-130 25 Tert-Butanol 33219-03 110 199 200 300 287 ug/L EPA 8260B 5125103 96.2 89.5 7.13 70-130 25 Methyl-t-Butyl Ether 33219-03 120 39.8 39.9 156 146 ug/L EPA 8260B 5125103 95.6 69.8 31.1 70-130 25 Benzene 33211-03 <0.50 40.0 40.0 39.6 39.4 ug/L EPA 8260B 5122103 99.0 98.6 0.506 70-130 25 Toluene 33211-03 <0.50 40.0 40.0 40.7 40.3 ug/L EPA 8260B 5/22103 102 101 1.06 70-130 25 Tert-Butanol 33211-03 <5.0 200 200 208 205 ug/L EPA 8260B 5122103 104 102 1.24 70-130 25 Methyl-t-Butyl Ether 33211-03 <0.50 40.0 40.0 45.4 45.1 ug/L EPA 8260B 5122103 114 113 0.817 70-130 25 Benzene 33234-17 <0.50 40.0 40.0 39.3 37.5 ug/L EPA 8260B 5123103 98.3 93.8 4.63 70-130 25 Toluene 33234-17 <0.50 40.0 40.0 41.9 40.4 ug/L EPA 8260B 5123103 105 101 3.62 70-130 25 Tert-Butanol 33234-17 <5.0 200 200 206 197 ug/L EPA 8260B 5123103 103 98.5 4.38 70-130 25 Methyl-t-Butyl Ether 33234-17 <0.50 40.0 40.0 37.2 36.5 ug/L EPA 8260B 5123103 93.0 91.2 1.90 70-130 25 I Approved By: J I Kiff . �KIFFANACAL, LLC • 2795 2nd St, Suite 300Oils, CA 95616 530-2974800 ��