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885 Jarvis Drive <br /> 'Sequoia Morgan Hill CA95037 <br /> (408)776-9600 <br /> 4 FAX(408)782-6308 <br /> Analytical www sequoialabs corn <br /> is <br /> Blaine Tech Services(Shell) Project 1267 Country Club <br /> 1680 Rogers Avenue Project Number 1267 Country Club/Stockton Reported <br /> San Jose CA,95112 Project Manager Nick Sudano 02/20/01 11 18 <br /> Industrial Solvents by EPA Method 8015 (modified) - Quality Control <br /> Sequoia Analytical -Morgan Hill <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch OL19034-EPA 3810 Heads ace <br /> Blank(OL I9034-BLKI) _ Prepared 12/20/00 Analyzed 12/21/00 <br /> Methanol ND 100 mg/l <br /> Surrogate 1 pentanol 530 500 106 55-157 <br /> Surrogate 1 pentanol(dbwax) 499 500 998 57-170 <br /> LCS(OL19034-BSI) _ Prepared 12/20/00 Analyzed 12/21/00 <br /> Methanol 755 100 mg/I 900 944 70-130 <br /> Surrogate I-pentanol 453 500 906 55-157 <br /> Surrogate 1 pentanol(dbwax) 508 500 102 57-170 <br /> Matrix Spike(OL19034-MSI) _ _ _ Source MJL0007-01 _Prepared 12/20/00 Analyzed 12/21/00 <br /> Methanol - 997 100 mg/] 800 _ 1 11 __111 50-1150 A _ <br /> gate I-pentanol 4 77 500 954 55-157 <br /> gate 1 pentanol(dbwa)j 534 500 107 57-170 <br /> Raatnx Spike Dup(OL19034-MiSDI) _ Source KiL0007-01 _ Prepared 12/20/00 Analyzed 12/21/00 <br /> Methanol _ 102 100 mg/1 800 1 11 114 50-150 228 _ 50 <br /> Surrogate I-pentanol 543 _ 500 109 55-157 <br /> Surrogate I-pentanol(dbwax) 607 500 121 57-170 <br /> Batch OL25004-EPA 3810 Heads ace <br /> Blank(OL25004-BLK1) Prepared&Analyzed 12/27/00 <br /> Methanol ND 100 mgt/ <br /> Surrogate I-pentanol 519 500 106 55-157 <br /> Surrogate I-pentanol(dbwax) 498 500 996 57-170 <br /> LCS(OL25004-BSI) Prepared&Analyzed 12/27/00 <br /> Methanol 690 100 mgt] 800 850 70-130 <br /> Surrogate 1 pentanol 451 500 901 55-157 <br /> Surrogate I-pentanol(dbwax) 409 500 818 57-170 <br /> ola Analytical-Morgan Hill The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document This analytical report must be reproduced in its entirety <br /> Page Page 12 of 14 <br />