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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Report <br /> Client: EMCON Associates Service Request: S941424 <br /> Project: TOSCO#11192/0952-090.02 Date Collected: 1119,10194 <br /> Sample Matrix: Soil Date Received: 11/11/94 <br /> Date Extracted: NA <br /> Halogenated Volatile Organic Compounds <br /> EPA Methods 5030/8010 <br /> Units: mg/Kg(ppm) <br /> As Received Basis <br /> Sample Name: 1.1192-THP3S-25 Method Blank <br /> Lab Code: S941424-008 5941115-SB <br /> Date Analyzed: 11/15/94 11/15/94 <br /> Analyte Mme' <br /> Dichlorodifluoromethane(CFC 12) 0.1 ND ND <br /> Chloromethane 0.1 ND ND <br /> Vinyl Chloride 0.05 ND NSD <br /> Bromomethane 0.05 ND <br /> 0.0.5 ND ND <br /> Chloroethane <br /> Trichlorofluoromethane(CFC 11) 0.05 ND ND <br /> 1,1 Dichloroethene 0.05 ND ND <br /> Trichlorotrifluoroethane(CFC 113) 0.05 ND ND <br /> Methylene Chloride 0.05 ND ND <br /> trans-l,2-Dichldroethene 0.05 ND ND <br /> cis-1,2-D ichloroethene 0.05 ND ND <br /> 1,1-Dichloroedme 0.05 ND ND <br /> ND <br /> 0.05 ND <br /> Chloroform <br /> 0.05 ND ND <br /> 1,1,1-Trichloroethane(TCA) <br /> Carbon Tetrachloride 0.05 ND ND <br /> 1,2-Dichloroethane 0.05 ND ND <br /> Trichloroethene(TCE) 0.05 ND NSD <br /> 1,2-Dichloropropane 0.05 ND <br /> Bromodichloromethane 0.05 ND ND <br /> 2-Chloroethyl Vinyl Ether 0.5 ND ND <br /> trans-1,3-Dichloropropene 0.05 ND ND <br /> cis-1,3-Dichloropropene 0.05 ND ND <br /> 1,1,2 Trichloroethane 0.05 ND ND <br /> Tetrachloroethene(PCE) 0.05 ND ND <br /> 0.05 ND ND <br /> D ibromochloromethane <br /> 0.05 ND ND <br /> Chlorobenzene <br /> ND <br /> 0.05 ND <br /> Bromoform <br /> 1,1,2,2-Tetrachloroethane 0.0.1 1 ND ND <br /> ND ND ., <br /> 1,3-Dichlorobenzene <br /> 1,4-Dichlorobenzene 0.1 ND ND <br /> 1,2-Dichlorobenzene 0.1 ND ND <br /> Date: �3•Al c <br /> Approved By: <br /> 354NO60196 <br /> Page 9 of 15 <br />