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819 Striker Ave Ste 8 Sequoia Sacrwnem,CA 95834 Analytical (9 -9600 FAX(916)92"100 www soquailuoialalabs cont Gettler-Ryan-Dublin Project TOSCO 11192,Stockton,CA 5305429 6747 Sierra Court,Ste J Project Number NIA Reported Dublin CA,94568 Project Manager Deanna L Harding 05/29/03 17 15 Volatile Organic Compounds by EPA Method 8260B Sequoia Analytical - Sacramento Reporting Analyte Result Limit Units Dilution Batch Prepared Analyzed Method Notes MW-8 5305429-08 Water Sam led 05/14/03 11 50 Received 05/15/03 16 40 Tert-butyl alcohol ND 100 ug/l 1 3050449 05/27/03 05/28/03 EPA 8260B Dr-isopropyl ether ND 2 0 Ethyl tert-butyl ether ND 20 " Tert-amyl methyl ether ND 20 Ethanol ND 500 1,2-Dichloroethane ND 20 ^ 1,2-Dibromoethane(EDB) ND 2 0 " Surrogate 1,2-DCA-d4 104% 60-140 MW-9(5305429-09)Water Sampled 05/14/031030 Received 05/15/0316 40 Tert-butyl alcohol ND 100 ug/l 1 3050449 05/27/03 05/28/03 EPA 8260B Di-isopropyl ether ND 2 0 ' " " Ethyl tert-butyl ether ND 20 1. " " Tert-amyl methyl ether ND 2 0 Ethanol ND 500 " 1,2-Dichloroethane ND 20 " 1,2-Dibromoethane(EDB) - ND 20 Surrogate 1,2-DCA-d4 I11 % 60-140 " MW-10($305429-1.0)Water Sampled 05/14/03 11 20 Received 05/15/03 16 40 Tert-butyl alcohol ND 100 ug/) 1 3050437 05/27/03 Y 05/28/03 EPA 8260B Di-isopropyl ether ND 20 " Ethyl tert-butyl ether ND 20 ^ " Tert-amyl methyl ether ND 2 0 Ethanol ND 500 " 1,2-Dichloroethane ND 2 0 1,2-Dibromoethane(EDB) ND 2 0 " Surrogate 1,2-DCA-d4 140% 60-140 " Sequoia Analytical- Sacramento The results in this report apply to the samples analyzed in accordance with the chain custody document Unless otherwise stated results are reported on a wet weight basis This analytical report must be reproduced in its entirety Page l 1 of 23