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TBC Laboratories, Inc <br /> TRC Alton Geoscience Project 11192 <br /> 21 Technology Drive Project Number [none] <br /> Irvine CA,92618-2302 Project Manager Anju Farfan Reported 09/12/05 14 35 <br /> Volatile Organic Analysis (EPA Method 8260) <br /> BCL Sample ID 0508601-02 FTiient Sample Name 11192, S-2, S-2, 8/26/2005 1145 OOAM, Ben Summersett <br /> Prep Run Instru- QC MIB Lab <br /> Constituent Result Units PQL MDI. Method Date Date/Time Analyst ment ID Dilution Batch ID Bias Quals <br /> Benzene 10 ug/L 2 5 0 60 EPA-8260 09/01/05 09/01/05 19 31 Irf MS-V9 5 B010046 NO A01 <br /> 1,2-Dibromoethane NO ug1L 2 5 0 55 EPA-8260 09/01/05 09/01105 1931 Irf MS-V9 5 B010046 NO A01 <br /> 1,2-Dichloroethane NO uglL 2 5 1 2 EPA-8260 09/01/05 09/01/05 1931 Irf MS-V9 5 8010046 NO A01 <br /> Ethylbenzene 470 ug/L 2 5 065 EPA-8260 09/01/05 09/01/05 1931 Irf MS-V9 5 8010046 NO A01 <br /> Methyl t butyl ether 24 uglL 2 5 075 EPA-8260 09/01/05 09/01/05 1931 Irf MS-V9 5 B010046 NO A01 <br /> Toluene 1 8 uglL 2 5 075 EPA-8260 09/01/05 09/01/05 1931 Irf MS-V9 5 8010046 ND A01, J <br /> Total Xylenes 360 uglL 60 2 0 EPA-8260 09/01/05 09/01/05 1931 Irf MS-V9 5 B010046 NO A01 <br /> t-Amy!Methyl ether NO uglL 2 5 1 6 EPA-8260 09/01/05 09/01105 1931 Irf MS-V9 5 B010046 ND A01 <br /> t-Butyl alcohol 1300 uglL 50 50 EPA-8260 09/01/05 09/01105 1931 Irf MS-V9 5 B010046 ND A01 <br /> Diwpropyl ether ND ug1L 2 5 1 2 EPA-8260 09/01/05 09/01/05 1931 Irf MS-V9 5 8010046 ND A01 <br /> Ethanol NO uglL 5000 550 EPA-8260 09/01/05 09/01/05 1931 Irf MS-V9 5 8010046 NO A01 <br /> Ethyl t-butyl ether NO uglL 2 5 1 4 EPA-8260 09/01/05 09/01/05 1931 Irf MS-V9 5 B010046 NO A01 <br /> Total Purgeable Petroleum 15000 uglL 500 230 EPA-8260 09/01/05 09/02/05 1438 Irf MS-V9 10 8010046 NO A01 <br /> Hydrocarbons <br /> 1 2-Dichloroethane-d4(Surrogate) 108 % 76-114 (LCL-UCL) EPA-8260 09/01/05 09/02/05 1438 Irf MS-V9 10 8010046 <br /> 1 2 Dichioroethane-d4(Surrogate) 94 4 % 76-114 (LCL-UCL) EPA-8260 09/01/05 09/01/05 1931 Irf MS-V9 5 8010046 <br /> Toluene-d8(Surrogate) 981 % 88-110 (LCL-UCL) EPA-8260 09/01/05 09/01/05 1931 Irf ALIS-V9 5 8010046 <br /> Toluene-dB(Surrogate) 98 3 % 88-110 (LCL-UCL) EPA-8260 09/01/05 09/02/05 1438 Irf MS-V9 10 B010046 <br /> — I <br /> 4_Bromofluorobenzene(Surrogate) 101 % 86-115 (LCL-UCL) EPA-8260 09/01/05 09/01/05 1931 Irf MS-V9 5 B010046 <br /> 4-Bromofluorobenzene(Surrogate) 924 % 86-116 (LCL-UCL) EPA-8260 09/01/05 09/02/05 1438 Irf MS-V9 10 B010046 W Y <br /> BC Laboratories The results in this report apply to the samples analyzed to accordance with the chain of custody document This analytical report must be reprocluced in its entirety <br /> . All results listed to this report are for the exclusive use of the submitting parry BC LaboratoneqJ11111purrics no responsibrhry,for report alteration separation detachment nr third para interpreranon - <br /> 4100 Atlas Court• Bakersfield,CA 93308• (67-4911 • FAX(661)327-1918•www bclabs com Page 4 of 12 <br />