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Table 4b SPLIT SAMPLES 8 OXYS by EPA Method 8260B FORMER SHELL SERVICE STATION 1267 Country Club Boulevard Date 1,2-DCA EDB TAME TBA DIPE ETBE ETHANOL Sampled (µg/l) (µg/l) (µg11) (µg/l) (µg/l} (µg/1) (µg/1) S-i 2/25/2005 ND<0 50 ND<0 50 ND<0 50 25 20 ND<0 50 ND<50 5/20/2005 ND<25 ND<25 ND<25 32 ND<25 ND<25 ND<250 S-2 TRC did not collect split samples during the Seccod Quarter 2005 event Results reported are those from the samples collected by Blame Tech on 5/20105 11/24/2004 ND<10 ND<10 ND<10 1.700 ND<20 ND<10 ND<1000 2/25/2005 ND<10 ND<10 ND<10 1700 ND<10 ND<10 ND<1000 5/20/2005 ND<10 n/a ND<10 1400 ND<10 ND<10 ND<1000 S-3 TRC did not collect split samples during the Seccod Quarter 2005 event Results reported are those from the samples collected by Blame Tech on 5120105 2/25/2005 8 4 ND<0 50 ND<0 50 ND<50 140 ND<0 50 ND<50 5/20/2005 63 ND<0 50 ND<0 50 ND<50 78 ND<0 50 ND<50 S-4 TRC did not collect split samples during the Seccod Quarter 2005 event Results reported are those from the samples collected by Blaine Tech on 5120105 2/25/2005 ND<0 50 ND<0 50 ND<0 50 ND<50 ND<0 50 ND<0 50 ND<50 5/20/2005 ND<0 50 n/a ND<0 50 ND<50 ND<0 50 ND<0 50 ND<50 TRC did not collect split samples during the Seccod Quarter 2005 event Results reported are those from the samples collected by Blame Tech on 5/20/05 S-5 11/24/2004 ND<20 ND<20 ND<20 1400 ND<40 ND<20 ND<2000 2/25/2005 ND<50 ND<50 71 130 ND<50 ND<50 ND<500 S-6 2/25/2005 ND<10 ND<10 18 ND<100 ND<10 ND<10 ND<1000 11192 Page 1 of I