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Report Number 40612 QC Report Matrix Spike/Matrix Spike Duplicate Date 10/21/2004 Project Name Sanchez Property Project Number Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Analyzed Recov Recov Diff Lima Limit Benzene 40617-01 <0 50 400 400 38 9 382 uglL EPA 8260B 10/19/04 974 956 1 82 70-130 25 Toluene 40617-01 <0 50 400 4D D 390 384 uglL EPA 8260B 10/19/04 975 960 1 63 70-130 25 Tert-Butanol 40617-01 <5 0 200 200 188 186 uglL EPA 8260B 10/19/04 943 931 1 27 70-130 25 Methyl-t-Butyl Ether40617-01 <0 50 400 400 354 361 uglL EPA 8260B 10/19/04 88 4 902 1 98 70-130 25 Benzene 40616-14 0 88 400 400 401 399 ug/L EPA 82606 10/20/04 982 977 0 492 70-130 25 Toluene 40616-14 <0 50 400 40 D 39 2 386 ug/L EPA 82606 10/20/04 98 1 964 1 74 70-130 25 Tert-Butanol 40616-14 1300 200 200 1560 1580 ug/L EPA 82606 10/20/04 110 125 126 70-130 25 Methyl-t-Butyl Ether 40616-14 84 400 40 D 120 119 ug/L EPA 8260B 10/20/04 908 879 327 70-130 25 Benzene 40654-02 051 400 40 0 41 0 408 ug/L EPA 8260B 10/20/04 101 101 D 570 70-130 25 Toluene 40654-02 <0 50 400 40 0 403 395 uglL EPA 82606 10/20/04 101 988 206 70-130 25 Tert-Butanol 40654-02 45 200 200 239 236 uglL EPA 8260B 10{20104 969 955 146 70-130 25 Methyl-t-Butyl Ether40654-02 26 400 40 0 615 616 uglL EPA 82606 10/20/04 89 0 892 0 189 70-130 25 Benzene 40318-05 <0 50 400 40o 399 388 uglL EPA 8260B 10/19/04 999 970 2 85 70-130 25 Toluene 40318-05 <0 50 400 400 397 384 uglL EPA 8260B 10/19/04 99 2 961 3 14 70-130 25 Tert-Butanol 40318-05 <5 0 200 200 207 205 uglL EPA 82606 10/19/04 103 103 0 666 70-130 25 Methyl-t-Butyl Ether 40318-05 <0 50 400 4011 429 424 uglL EPA 82608 10/19/04 107 106 1 03 70-130 25 Benzene 40622-12 <0 50 400 400 405 392 ug/L EPA 82606 10/19/04 101 980 3 17 70-130 25 Toluene 40622-12 <0 50 400 400 402 391 ug1L EPA 8260B 10/19/04 100 977 274 70-130 25 i I � KIFF ANALYTICAL, LLC Approved By Joe Mfr 2795 2nd St, Suite 300 Davis, CA 95616 530-2974800